首页> 外文期刊>Vacuum: Technology Applications & Ion Physics: The International Journal & Abstracting Service for Vacuum Science & Technology >Photocatalytic activity of nanostructured TiO{sub}2 thin films prepared by dc magnetron sputtering method
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Photocatalytic activity of nanostructured TiO{sub}2 thin films prepared by dc magnetron sputtering method

机译:直流磁控溅射法制备纳米结构TiO {sub} 2薄膜的光催化活性

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摘要

Transparent and colourless nanostructured titanium dioxide thin films have been fabricated on microscope glass slides by the dc magnetron reactive sputtering method using Ar and O{sub}2 as working gases. X-ray diffraction (XRD), Xray photoelectron spectroscopy (XPS) and UV-Vis-NIR spectrophotometer technologies were used to characterize the films. The stoichiometric TiO{sub}2 thin films with anatase phase were obtained by optimizing the sputtering parameters such as sputtering gas Ar : 0{sub}2 ratio, sputtering gas pressure and sputtering power. The photocatalytic activity of the samples was tested on the degradation of Rhodamine B(Rh.B) dye. The relatively better degradation efficiency compared with Rh.B mineralization was obtained in the sample annealed at 5000C.
机译:通过使用Ar和O {sub} 2作为工作气体的直流磁控反应溅射法在显微镜载玻片上制备了透明无色的纳米结构二氧化钛薄膜。使用X射线衍射(XRD),X射线光电子能谱(XPS)和UV-Vis-NIR分光光度计技术来表征薄膜。通过优化溅射参数,例如溅射气体Ar:0 {sub} 2的比例,溅射气压和溅射功率,获得了具有锐钛矿相的化学计量的TiO {sub} 2薄膜。测试了样品对罗丹明B(Rh.B)染料降解的光催化活性。与在5000℃退火的样品相比,Rh.B矿化具有相对更好的降解效率。

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