Metallation of Calix (4) arene with Thulium Diiodide, TmI_2(DME)_3: Molecular Structure of ((5, 11, 17, 23-Tetra-tert-butyl-25, 27-dioxo-26, 28-dimethoxycalix (4) arene) thulium (III) iodide (diethyl etherate))

Igor L. Fedushkin; Marc Weydert; Anatoly A. Fagin; Sergei E. Nefedov; Igor L. Eremenko; Mikhail N. Bochkarev; Herbert Schumann

首页> 外文期刊>Zeitschrift fur Naturforschung, B. A Journal of Chemical Sciences >Metallation of Calix (4) arene with Thulium Diiodide, TmI_2(DME)_3: Molecular Structure of ((5, 11, 17, 23-Tetra-tert-butyl-25, 27-dioxo-26, 28-dimethoxycalix (4) arene) thulium (III) iodide (diethyl etherate))

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Metallation of Calix (4) arene with Thulium Diiodide, TmI_2(DME)_3: Molecular Structure of ((5, 11, 17, 23-Tetra-tert-butyl-25, 27-dioxo-26, 28-dimethoxycalix (4) arene) thulium (III) iodide (diethyl etherate))

机译：用二碘化，TmI_2（DME）_3对杯（4）芳烃进行金属化：（（（5，11，17，23-四叔丁基25，27-二氧-26，28-二甲氧基杯（4）芳烃）碘化th（III）（乙醚）

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[(5, 11, 17, 23-Tetra-tert-butyl-25, 27-dioxo-26, 28-dimethoxycalix [4] arene) thulium (III) iodide (diethyl etherate)] 1 is obtained by deprotonation of 5, 11, 17, 23-tetra-tert-butyl-25, 27-dihydroxy-26, 28-dimethoxy-calix [4] arene with 2 equivalents of TmI_2 (DME)_3 in THF.

机译：[（5、11、17、23-四叔丁基-25、27-二氧代-26、28-二甲氧基杯[4]芳烃）碘化ul（III）（二乙基醚化物）] 1通过将5脱质子化而获得11、17、23-四叔丁基-25、27-二羟基-26、28-二甲氧基-杯[4]芳烃，其中含2当量的TmI_2（DME）_3在THF中。

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《Zeitschrift fur Naturforschung, B. A Journal of Chemical Sciences》 |1999年第4期|共3页
作者
Igor L. Fedushkin; Marc Weydert; Anatoly A. Fagin; Sergei E. Nefedov; Igor L. Eremenko; Mikhail N. Bochkarev; Herbert Schumann;
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正文语种 eng
中图分类化学;
关键词
thulium diiodide; calix arene;

机译：二碘化;杯芳烃;

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1. Metallation of Calix (4) arene with Thulium Diiodide, TmI_2(DME)_3: Molecular Structure of ((5, 11, 17, 23-Tetra-tert-butyl-25, 27-dioxo-26, 28-dimethoxycalix (4) arene) thulium (III) iodide (diethyl etherate)) [J] . Igor L. Fedushkin, Marc Weydert, Anatoly A. Fagin, Zeitschrift fur Naturforschung, B. A Journal of Chemical Sciences . 1999,第4期

机译：用二碘化，TmI_2（DME）_3对杯（4）芳烃进行金属化：（（（5，11，17，23-四叔丁基25，27-二氧-26，28-二甲氧基杯（4）芳烃）碘化th（III）（乙醚）
2. Yttrium complexes derived from 5,11,17,23-tetra-tert-butyl-25,27-dihydroxy-26,28-dimethoxycalix[4]arene (LH_2).Synthesis,properties,and structures [J] . A.A.Trifonov, E.A.Fedorova, G.K.Fukin, Russian Chemical Bulletin . 2003,第12期

机译：由5,11,17,23-四叔丁基-25,27-二羟基-26,28-二甲氧基杯[4]芳烃（LH_2）衍生的钇配合物。合成，性质和结构
3. [5,11,17,23-Tetra-tert-butyl-25,27-(3,6-dioxaoctan-1,8-dioxy)-26,28-bis(pyridin-2-ylmethoxy)calix[4]arene]sodium iodide–1,2,4,5-tetrafluoro-3,6-diiodobenzene–methanol (2/3/4) [J] . Cavallo G., Metrangolo P., Parisi M.F., Acta Crystallographica Section E: Crystallographic Communications . 2013,第5期

机译：[5,11,17,23-四叔丁基-25,27-（3,6-dioxaoctan-1,8-dioxy）-26,28-双（吡啶-2-基甲氧基）杯[4]芳烃碘化钠–1,2,4,5-四氟-3,6-二碘苯–甲醇（2/3/4）
4. 5,11,17,23-Tetra-tert-butyl-25,26,27,28-tetrapropynyloxy-2,8,14,20-tetrathiacalix[4]arene [O] . Xiong Li, Hong-Wei Han, Xiang-Gao Meng 2016

机译：5,11,17,23-四叔丁基-25,26,27,28-四炔氧基-2,8,14,20-四杂杯[4]芳烃
5. [5,11,17,23-Tetra-tert-butyl-25,27-(3,6-dioxaoctan-1,8-dioxy)-26,28-bis(pyridin-2-ylmethoxy)calix[4]arene]sodium iodide–1,2,4,5-tetrafluoro-3,6-diiodobenzene–methanol (2/3/4) [O] . Gabriella Cavallo, Pierangelo Metrangolo, Melchiorre F. Parisi, 2013

机译：[5,11,17,23-四叔丁基-25,27-（3,6-dioxaoctan-1,8-dioxy）-26,28-双（吡啶-2-基甲氧基）杯[4]芳烃碘化钠–1,2,4,5-四氟-3,6-二碘苯–甲醇（2/3/4）

Metallation of Calix (4) arene with Thulium Diiodide, TmI_2(DME)_3: Molecular Structure of ((5, 11, 17, 23-Tetra-tert-butyl-25, 27-dioxo-26, 28-dimethoxycalix (4) arene) thulium (III) iodide (diethyl etherate))

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