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Highly crystalline graphene oxide nano-platelets produced from helical-ribbon carbon nanofibers

机译:由螺旋带状碳纳米纤维制成的高度结晶的氧化石墨烯纳米片

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摘要

Graphene oxide nano-platelets were produced from helical-ribbon carbon nanofibers by oxidation with KMnO4/H2SO4 and further exfoliation by ultrasonication. The KMnO4 to carbon nanofiber ratio is 1:1. TEM and AFM were used to characterize the samples. TEM shows individual nanocrystals with straight edges and SAED yields a hexagonal spot pattern arrangement, attributed to graphene layers. The thickness of the nanocrystals, measured by AFM, is approximately 1.7 ran, which corresponds to a single layer of hydrated graphene oxide.
机译:通过用KMnO4 / H2SO4氧化并通过超声进一步剥离,由螺旋状碳纳米纤维制成氧化石墨烯纳米片。 KMnO4与碳纳米纤维的比例为1:1。 TEM和AFM用于表征样品。 TEM显示出具有直边缘的单个纳米晶体,并且SAED产生了六边形斑点图案排列,这归因于石墨烯层。通过AFM测量的纳米晶体的厚度为约1.7nm,其对应于单层的水合氧化石墨烯。

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