Size-exclusion chromatography study of the molecular-weight distribution of gamma-irradiated pullulan

Shingel KI.; Petrov PT.; Tsarenkov VM.

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Size-exclusion chromatography study of the molecular-weight distribution of gamma-irradiated pullulan

机译：尺寸排阻色谱法研究γ-辐照支链淀粉的分子量分布

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The polyelectrolyte behavior of gamma-irradiated pullulan in aqueous solutions leads to secondary effects of adsorption on a Shodex OHPak KB 806 column gel during size-exclusion chromatography. Suppression of the polyelectrolyte properties of gamma-irradiated pullulan is achieved by using a 0.05 M aqueous solution of NaH2PO4 (pH 4.95) as the mobile phase. Under these conditions, adequate molecular-weight distributions of gamma-irradiated pullulan samples are obtained. (C) 2000 Elsevier Science Ltd. All rights reserved. [References: 17]

机译：在大小排阻色谱过程中，γ射线辐照的支链淀粉在水溶液中的聚电解质行为导致其在Shodex OHPak KB 806色谱柱凝胶上的吸附产生次级影响。通过使用0.05 M的NaH2PO4（pH 4.95）水溶液作为流动相，可以抑制γ-辐照的支链淀粉的聚电解质性能。在这些条件下，可以获得足够的分子量分布的伽马射线辐照的支链淀粉样品。（C）2000 Elsevier ScienceLtd。保留所有权利。 [参考：17]

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《Carbohydrate research》 |2000年第4期|共5页
作者
Shingel KI.; Petrov PT.; Tsarenkov VM.;
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正文语种 eng
中图分类糖（醣）;有机化学;
关键词
Gamma-irradiated pullulan; High-performance size-exclusion chromatography; Molecular-weight distribution; Viscosity; Dilute;

机译：γ射线支链淀粉;高效排阻色谱法;分子量分布;粘度;稀;

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1. Size-exclusion chromatography study of the molecular-weight distribution of gamma-irradiated pullulan [J] . Shingel KI., Petrov PT., Tsarenkov VM. Carbohydrate research . 2000,第4期

机译：尺寸排阻色谱法研究γ-辐照支链淀粉的分子量分布
2. Report on the cooperative determination of molecular-weight averages of polymers by size-exclusion chromatography V.Dependence of molecular weight averages on detectors and mobile phases [J] . S.Mori, S.Takayama, Y.Goto 分析化学 . 1997,第1期

机译：尺寸排阻色谱法协同测定聚合物分子量平均值的报告V.分子量平均值对检测器和流动相的依赖性
3. Report on the cooperative determination of the molecular-weight averages of polymers by size-exclusion chromatography VI. A report on a third round-robin test [J] . M.Nagata, S.Mori, Y.Goto 分析化学 . 1997,第2期

机译：报告通过尺寸排阻色谱法VI协同测定聚合物的分子量平均值。第三次循环测试的报告
4. Molecular Composition Study of Mumijo from Different Geographic Areas Using Size-Exclusion Chromatography, NMR Spectroscopy, and High-Resolution Mass-Spectrometry [C] . A.I.Konstantinov, G.N.Vladimirov, A.S.Grigoryev, Functions of natural organic matter in changing environment . 2012

机译：使用尺寸排阻色谱，NMR光谱和高分辨率质谱研究不同地理区域的Mumijo的分子组成
5. Size-exclusion chromatography with refractometric and viscometric detection to determine the solution conformational entropy of mono-, di-, and oligosaccharides [D] . Morris, Mallory J. 2013

机译：尺寸排阻色谱，通过折光和粘度检测确定单糖，二糖和寡糖的溶液构象熵
6. High-performance size-exclusion chromatography studies on the formation and distribution of polar compounds in camellia seed oil during heating [O] . Hong-xia Feng, Rokayya Sam, Lian-zhou Jiang, 2016

机译：高效排阻色谱法研究山茶籽油加热过程中极性化合物的形成和分布
7. Report on the cooperative determination of the molecular-weight averages of polymers by size-exclusion chromatography VI. A report on a third round-robin test. [O] . M. NAGATA, S. MORI, Y. GOTO, 1997

机译：尺寸排阻色谱vi的分子量平均值的协同测定报告。关于第三轮罗宾试验的报告。

Size-exclusion chromatography study of the molecular-weight distribution of gamma-irradiated pullulan

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