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Synthesis and characterisation of sol-gel derived nanostructured composite of ZnO/PVD thin films

机译:溶胶-凝胶法制备的ZnO / PVD薄膜纳米结构复合材料的表征

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摘要

Pure ZnO films and ZnO nanoparticle dispersed polyvinylpyrrolidone (PVP) films were prepared on a Pyrex glass substrate by sol-gel dip coating using a zinc acetate precursor. The thin film is extensively characterised for its surface morphology, chemistry, thickness and nanocrystallite size, using various advanced analytical techniques such as SEM, Fourier transform infrared spectroscopy, X-ray photoelectron spectroscopy and atomic force microscopy. Under the given processing conditions, ZnO semiconductor thin films with nanocrystallite size 20-30 nm were obtained, and the ZnO nanoparticle size in the PVP matrix increased with increase in ZnO content.
机译:通过使用醋酸锌前体的溶胶-凝胶浸涂在Pyrex玻璃基板上制备纯ZnO薄膜和ZnO纳米颗粒分散的聚乙烯吡咯烷酮(PVP)薄膜。使用各种先进的分析技术,例如SEM,傅里叶变换红外光谱,X射线光电子能谱和原子力显微镜,可以对薄膜的表面形貌,化学性质,厚度和纳米微晶尺寸进行广泛表征。在给定的工艺条件下,获得了纳米晶体尺寸为20-30 nm的ZnO半导体薄膜,随着ZnO含量的增加,PVP基体中的ZnO纳米颗粒尺寸也随之增加。

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