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Crystallinity improvement of hydroxyapatite coating by saturated steam treatment

机译:通过饱和蒸汽处理提高羟基磷灰石涂层的结晶度

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摘要

During plasma spraying, partial hydroxyapatite (HA) decomposes and partial constituent of the coatings transforms into amorphous phase, which greatly reduce the crystalline HA content of the coatings. Experimental results indicate that the content of crystalline HA in the coatings can be increased significantly by saturated steam treatment. Owing to the existence of steam, the reaction [3Ca(3)(PO4)(2)+CaO+H2O -> Ca-10(PO4)(6)(OH)(2)] will take place during treatment, and with the increase in processing temperature and the increase in holding period, the content of the crystalline HA increases obviously. In addition, HA nanocrystals can be obtained with suitable processing parameters.
机译:在等离子喷涂过程中,部分羟基磷灰石(HA)分解,涂层的部分成分转变为无定形相,这大大降低了涂层的结晶HA含量。实验结果表明,通过饱和蒸汽处理可以显着增加涂层中结晶HA的含量。由于存在蒸汽,在处理过程中将发生[3Ca(3)(PO4)(2)+ CaO + H2O-> Ca-10(PO4)(6)(OH)(2)]反应。随着加工温度的升高和保温时间的增加,结晶态HA的含量明显增加。另外,可以以合适的加工参数获得HA纳米晶体。

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