Synthesis of Optically Active Deuterated Primary Amines via Reduction of N-tert-Butanesulfinyl Aldimines

Mao Liu; Ying Xie; Jing Li; Hongjie Pan; Hua Tian; Yian Shi

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Synthesis of Optically Active Deuterated Primary Amines via Reduction of N-tert-Butanesulfinyl Aldimines

机译：通过还原N-叔丁烷亚磺酰基醛亚胺合成旋光的氘代伯胺

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摘要

Optically active deuterated primary amines have been obtained with 78?98% ee's from chiral N-tert-butanesulfinyl aldimines via reduction with NSelectride and subsequent alcoholysis.

机译：通过用NSelectride还原并随后进行醇解反应，从手性N-叔丁烷亚磺酰基醛亚胺中获得了78〜98％ee的旋光性氘代伯胺。

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《The Journal of Organic Chemistry》 |2014年第17期|共5页
作者
Mao Liu; Ying Xie; Jing Li; Hongjie Pan; Hua Tian; Yian Shi;
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原文格式 PDF
正文语种 eng
中图分类有机化学;
关键词
Synthesis; Primary; Aldimines;

机译：合成;主要;亚胺;

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专利

1. Synthesis of Optically Active Deuterated Primary Amines via Reduction of N-tert-Butanesulfinyl Aldimines [J] . Mao Liu, Ying Xie, Jing Li, The Journal of Organic Chemistry . 2014,第17期

机译：通过还原N-叔丁烷亚磺酰基醛亚胺合成旋光的氘代伯胺
2. Convenient synthesis of optically active deuterated primary alcohols via deuteride reduction of acetals derived from homochiral (1R*,2R*)-3,3,3-trifluoro-1-phenylpropane-1,2-diols [J] . Morelli Carlo F., Cairoli Paola, Marigolo Tiziana, Tetrahedron, Asymmetry: The International Journal for Repid Publication on all Aspects of Asymmetry in Orgainc, Inorganic, Organometallic, Physical and Bio-Organic Chemistry . 2009,第3期

机译：通过氘化缩合衍生自同手性（1R *，2R *）-3,3,3-三氟-1-苯基丙烷-1,2-二醇的缩醛的缩醛方便合成旋光的氘代伯醇
3. Asymmetric Synthesis Of α-branched Allylic Amines By The Rh(i)-catalyzed Addition Of Alkenyltrifluoroborates To N-tert-butanesulfinyl Aldimines [J] . Katrien Brak, Jonathan A. Ellman Journal of the American Chemical Society . 2009,第11期

机译：Rh（i）催化烯基三氟硼酸酯加成至N-叔丁烷亚磺酰基Aldimines的α-支链烯丙基胺的不对称合成
4. Synthesis and characterisation of optically active and water soluble carbon nano particles by chemical reduction method [C] . Shivaramakrishnan K., Namasivayam Karthik Raja, Aswin Lakshmi Narashiman, 2013 International Conference on Advanced Nanomaterials and Emerging Engineering Technologies . 2013

机译：光学活性和水溶性碳纳米粒子的化学还原法合成与表征
5. Hydrozirconation/zirconium-zinc transmetalation/aldimine addition: One-pot synthesis of allylic, c-cyclopropylalkyl, and homoallylic amine from alkynes. [D] . Kendall, Christopher Nicholas Owen. 2004

机译：加氢锆/锆锌金属转移/醛亚胺的添加：从炔烃一锅法合成烯丙基，c-环丙基烷基和均烯丙基胺。
6. Asymmetric Synthesis of Nonracemic Primary Amines via Spiroborate Catalyzed Reduction of pure (E)- and (Z)-O-Benzyloximes: Applications toward the Synthesis of Calcimimetic Agents [O] . Wenhua Ou, Sandraliz Espinosa, Héctor J. Meléndez, -1

机译：通过螺硼酸酯催化还原纯（E）-和（Z）-O-苄基肟的非外消旋伯胺的不对称合成：在拟钙剂合成中的应用
7. Indium-Mediated Asymmetric Barbier-Type Allylation of Aldimines in Alcoholic Solvents: Synthesis of Optically Active Homoallylic Amines [O] . -1

机译：铟介导的含酒精溶剂中醛胺的非对称倒钩型烯丙基：光学活性官胺的合成
8. Alkylation of Amines: A New Method for the Synthesis of Quaternary Ammonium Compounds from Primary and Secondary Amines [R] . Sommer, H. Z., Jackson, L. L. 1969

机译：胺的烷基化：从伯胺和仲胺合成季铵化合物的新方法

Synthesis of Optically Active Deuterated Primary Amines via Reduction of N-tert-Butanesulfinyl Aldimines

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