15,16-Epoxy-3,13(16),14-Neoclerodatrien-17,12:18,19-diolide, a new compound from Galatella punctata

Adekenov S.M.; Shults E.E.; Gatilov Yu.V.; Lomzov A.A.; Atazhanova G.A.; Kupriyanov A.N.

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15,16-Epoxy-3,13(16),14-Neoclerodatrien-17,12:18,19-diolide, a new compound from Galatella punctata

机译：15,16-Epoxy-3,13（16），14-Neoclerodatrien-17,12：18,19-diolide，一种来自Galatella punctata的新化合物

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摘要

The clerodane-type diterpenoid 5S,8R,9R,10R,12S-15,16-epoxy-3,13(16),14- neoclerodatrien-17,12:18,19diolide was isolated during a chemical study of the aerial part of the terrestrial plant Galatella punctata. Its structure was elucidated using IR, PMR, and ~(13)C NMR spectroscopy. The crystal and molecular structure of this diterpene was determined by an x-ray crystal structure analysis; the absolute configuration, by optical circular dichroism.

机译：在对甲虫的地上部分进行化学研究期间，分离出了环戊烷型二萜5S，8R，9R，10R，12S-15,16-环氧-3,13（16），14-新核黄三烯-17,12：18,19陆生植物Galatella punctata。使用IR，PMR和〜（13）C NMR光谱阐明了其结构。通过X-射线晶体结构分析确定该二萜的晶体和分子结构。通过光学圆二色性的绝对配置。

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来源
《Chemistry of Natural Compounds 》 |2013年第6期| 共4页
作者
Adekenov S.M.; Shults E.E.; Gatilov Yu.V.; Lomzov A.A.; Atazhanova G.A.; Kupriyanov A.N.;
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正文语种 eng
中图分类化学 ;
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γ- and δ-lactone; clerodane diterpenoid; Galatella punctata (Waldst. amp; Kit.) Nees (Asteraceae); NMR spectroscopy; optical circular dichroism; x-ray crystal structure analysis;

机译：γ-内酯和δ-内酯;聚环戊烷二萜;Galatella punctata（Waldst。＆Kit。）Nees（菊科）;NMR光谱;光学圆二色性;x射线晶体结构分析;

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1. 15,16-Epoxy-3,13(16),14-Neoclerodatrien-17,12:18,19-diolide, a new compound from Galatella punctata [J] . Adekenov S.M., Shults E.E., Gatilov Yu.V., Chemistry of Natural Compounds . 2013 ,第6期

机译：15,16-Epoxy-3,13（16），14-Neoclerodatrien-17,12：18,19-diolide，一种来自Galatella punctata的新化合物
2. 16-Hydroxycleroda-3,13-dien-15,16-olide induces anoikis in human renal cell carcinoma cells: involvement of focal adhesion disassembly and signaling [J] . Yu-Chi Chen, Bu-Miin Huang, Wei-Chang Lee, OncoTargets and therapy . 2018 ,第4期

机译：16-Hydroxycleroda-3,13-dien-15,16-内酰胺诱导人肾癌细胞的失神经：黏着斑的分解和信号传导
3. R and S )-phenylamino-cleroda-3,13(14), Z -dien-15,16 olide ( PGEA-AN ) inhibits the growth and cell survival of human neuroblastoma cell line SH-SY5Y by modulating P53 pathway [J] . Syed Saad Hussain, Kinza Rafi, Shaheen Faizi, Molecular and Cellular Biochemistry: An International Journal for Chemical Biology . 2018 ,第1a2期

机译：R和S）-phenylamino-cleroda-3,13（14），z -dien-15,16 olide（pgea-a）通过调节p53途径来抑制人神经母细胞瘤细胞系Sh-sh-sy5y的生长和细胞存活
4. The evaluation of flowability and wire sweep by epoxy molding compound for power module packages using Moldflow#x2122; [C] . Lee Taekkeun, Lim Aimee, Ko Youngsun, International Conference on Thermal, Mechanical and Multi-Physics Simulation and Experiments in Microelectronics and Microsystems . 2013

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5. 446a6b111214b-Heptamethyl-16-oxo-12344a566a6b78910111212a14a14b-octadecahydro-12b8a-(epoxymethano)picen-3-yl acetate [O] . Mohammad Nisar, Sajid Ali, M. Nawaz Tahir, 2013

机译：446a6b111214b-七甲基-16-氧代-12344a566a6b789101112 12a14a14b-十八烷基氢化物12b8a-（环氧甲氧基）乙酸3-甲基戊酯
6. Synthetic Studies on Terpenoid Compounds. XXXIII. A Total Synthesis of (±)-15,16-Epoxy-cis-cleroda-3,13(16),14-triene [O] . Takashi Tokoroyama, Reizo Kanazawa, Satoru Yamamoto, 1990

机译：萜类化合物的合成研究。 xxxiii。总合成（±）-15,16-环氧-CIS-CLERODA-3,13（16），14-三烯
7. Complete Fusion Leading to exp 32 S Compound Nucleus Via the exp 20 Ne + exp 12 C and exp 16 O + exp 16 O Entrance Channels [R] . Conjeaud, M., Harar, S., Saint-Laurent, F., 1977

机译：通过exp 20 Ne + exp 12 C和exp 16 O + exp 16 O入口通道完成Fusion到exp 32 s复合核的融合

15,16-Epoxy-3,13(16),14-Neoclerodatrien-17,12:18,19-diolide, a new compound from Galatella punctata

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