Substituent Effects on the Spectroscopic and Structural Parameters of Several New 1,3,2-Diazaphosphorinanes.Syntheses,Spectroscopic Characterization,and X-ray Crystallography

Khodayar Gholivand; Zahra Shariatinia; Fariba Yaghmaian

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Substituent Effects on the Spectroscopic and Structural Parameters of Several New 1,3,2-Diazaphosphorinanes.Syntheses,Spectroscopic Characterization,and X-ray Crystallography

机译：取代基对几种新的1,3,2-二氮杂磷酰肼的光谱和结构参数的影响。合成，光谱表征和X射线晶体学

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New 1,3,2-diazaphosphorinanes with the formula 4-X-C_6H_4NHP(O)[NH(CH_2)_3NH] (X=F (1),Cl (2),Br (3),and I (4)) were synthesized and characterized by ~1H,~(13)C,and ~(31)PNMR and IR spectroscopy,and elemental analysis.The structures have been determined for compounds 3 and 4 by X-ray crystallography.

机译：分子式为4-X-C_6H_4NHP（O）[NH（CH_2）_3NH]（X = F（1），Cl（2），Br（3）和I（4）的新1,3,2-二氮杂膦酰基通过〜1H，〜（13）C，〜（31）PNMR和IR光谱及元素分析合成并表征。通过X射线晶体学确定化合物3和4的结构。

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《Bulletin of the Chemical Society of Japan》 |2006年第10期|共3页
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Khodayar Gholivand; Zahra Shariatinia; Fariba Yaghmaian;
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1. Substituent Effects on the Spectroscopic and Structural Parameters of Several New 1,3,2-Diazaphosphorinanes.Syntheses,Spectroscopic Characterization,and X-ray Crystallography [J] . Khodayar Gholivand, Zahra Shariatinia, Fariba Yaghmaian Bulletin of the Chemical Society of Japan . 2006,第10期

机译：取代基对几种新的1,3,2-二氮杂磷酰肼的光谱和结构参数的影响。合成，光谱表征和X射线晶体学
2. The first naphthodiazaphosphorinane in the solid phase; Syntheses, spectroscopic studies and X-ray crystallography of some new 1,3,2- diheterophosphorus compounds [J] . Gholivand K., Shariatinia Z., Ansar S., Structural Chemistry . 2009,第3期

机译：固相中的第一种萘二氮杂正膦烷;一些新的1,3,2-二杂磷化合物的合成，光谱研究和X射线晶体学
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Substituent Effects on the Spectroscopic and Structural Parameters of Several New 1,3,2-Diazaphosphorinanes.Syntheses,Spectroscopic Characterization,and X-ray Crystallography

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