EFFECT OF REACTION SOLVENT ON THE HYDROGENATION OF ISOPHTHALONITRILE FOR META-XYLYLENDIAMINE PREPARATION

Sung Wook Row; Tae Young Chae; Kye Sang Yoo

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EFFECT OF REACTION SOLVENT ON THE HYDROGENATION OF ISOPHTHALONITRILE FOR META-XYLYLENDIAMINE PREPARATION

机译：反应溶剂对异戊二腈加氢制备间二甲苯二胺的影响

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摘要

This study focused on the effects of reaction solvent on the hydrogenation of isophthalonitrile (1PN) to produce m-Xylylenediamine (MXDA) over Ni-based commercial catalyst.The hydrogenation was carried out using various reaction solvents such as 1-methylimidazote,mesityiene,benzyl ether and isopropanol under various reaction conditions.It was observed that 1-methylimiazole outperformed the other reaction solvent,exhibiting a high MXDA yield and producing a low concentration of undesirable products.

机译：本研究着重研究了反应溶剂对间苯二甲腈（1PN）氢化在镍基商业催化剂上生产间苯二甲胺（MXDA）的影响。在不同的反应条件下，我们发现1-甲基咪唑的性能优于另一种反应溶剂，MXDA的收率高，不良产物的浓度低。

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来源
《The Canadian Journal of Chemical Engineering》 |2007年第6期|共4页
作者
Sung Wook Row; Tae Young Chae; Kye Sang Yoo;
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正文语种 eng
中图分类化学工业;
关键词
m-xylylenediamine (MXDA); reaction solvent; isophthalonitrile (IPN); hydrogenation;

机译：间苯二甲胺（MXDA）;反应溶剂;间苯二甲腈（IPN）;加氢;

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专利

1. EFFECT OF REACTION SOLVENT ON THE HYDROGENATION OF ISOPHTHALONITRILE FOR META-XYLYLENDIAMINE PREPARATION [J] . Sung Wook Row, Tae Young Chae, Kye Sang Yoo The Canadian Journal of Chemical Engineering . 2007,第6期

机译：反应溶剂对异戊二腈加氢制备间二甲苯二胺的影响
2. Hydrogenation of Isophthalonitrile with 1-Methylimidazole as an Effective Solvent for m-Xylenediamine Production [J] . Do Weon Lee, Kye Sang Yoo, Sang Duek Lee, Bulletin of the Korean Chemical Society . 2006,第3期

机译：1-甲基咪唑作为间苯二甲胺生产有效溶剂的间苯二甲腈加氢反应
3. Kinetic Solvent Effects on the Reactions of the Cumyloxyl Radical with Tertiary Amides. Control over the Hydrogen Atom Transfer Reactivity and Selectivity through Solvent Polarity and Hydrogen Bonding [J] . Salamone Michela, Mangiacapra Livia, Bietti Massimo The Journal of Organic Chemistry . 2015,第2期

机译：动力学溶剂对甲酰氧基自由基与叔酰胺反应的影响。通过溶剂极性和氢键控制氢原子转移反应性和选择性
4. Studies of Reaction Kinetics of Catalytic Hydrogenation of Isophthalonitrile for Meta-Xylenediamine Preparation [C] . Yugang Li, Lingqi Kong International Conference on Advances in Materials . 2015

机译：荟萃二甲腈催化氢化反应动力学研究荟萃二甲二胺制剂
5. Theoretical Insights in to the Influence of the Solvent on Heterogeneous Catalytic Hydrogenation and Hydrogenolysis Reactions. [D] . Sinha, Nishant K. 2011

机译：溶剂对非均相催化加氢和氢解反应影响的理论见解。
6. How Solvent Affects C–H Activation and HydrogenProduction Pathways in Homogeneous Ru-Catalyzed Methanol DehydrogenationReactions [O] . Vivek Sinha, §, Nitish Govindarajan, -1

机译：溶剂如何影响C–H活化和氢均相Ru催化甲醇脱氢的生产途径。反应
7. Sugar-Based Natural Deep Eutectic Mixtures as Green Intercalating Solvents for High-Yield Preparation of Stable MoS2 Nanosheets: Application to Electrocatalysis of Hydrogen Evolution Reaction [O] . -1

机译：基于糖的天然深凝胶混合物作为绿色插入溶剂，用于高产稳定的MOS2纳米晶片：氢分析氢进化反应的应用
8. Reactions of atomic hydrogen in water: solvent and isotope effects [R] . Bartels, D. M. 1999

机译：原子氢在水中的反应：溶剂和同位素效应

EFFECT OF REACTION SOLVENT ON THE HYDROGENATION OF ISOPHTHALONITRILE FOR META-XYLYLENDIAMINE PREPARATION

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