Direct ICF-MS determination of trace and ultratrace elements in geological materials after decomposition in a microwave oven. Part II. Quantisation of Ba, Cs, Ga, Hf, In, Mo, Nb, Pb, Rb, Sn, Sr, Ta and T1

J.G. Sen Gupta; N.B. Bertrand

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Direct ICF-MS determination of trace and ultratrace elements in geological materials after decomposition in a microwave oven. Part II. Quantisation of Ba, Cs, Ga, Hf, In, Mo, Nb, Pb, Rb, Sn, Sr, Ta and T1

机译：ICF-MS在微波炉中分解后直接测定地质材料中的痕量和超痕量元素。第二部分Ba，Cs，Ga，Hf，In，Mo，Nb，Pb，Rb，Sn，Sr，Ta和T1的量化

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A new method has been developed for the rapid determination of traces of Ba, Cs. Ga, Hf, In, Mo, Nb, Pb, Rb, Sn, Sr, Ta and Tl in silicate rocks and lake, stream and river sediments. The method involved dissolution of samples in a microwave oven by heating in a pressure decomposition Teflon vessel with a mixture of HF + HNO_3 + HC1 + H_3BO_3 + EDTA followed by direct rnukietement determination using inductively coupled plasma-mass spectrometry (TCP/MS). The method is faster than conventional dissolution of samples by open vessel acid digestion and fusion and determination by instrumental methods. The accuracy and precision of the developed method were tested by replicate analyses of a number of international geochemical reference samples of established trace element contents. Satisfactory correlation with the "recommended'' or "consensus" values was found and recoveries were in most cases 95-100%. New values for Ga, In, Nb and Tl in several international geochemieai reference materials are first reported in this paper.

机译：已经开发出一种新方法，用于快速测定痕量的Ba，Cs。硅酸盐岩石，湖泊，河流和河流沉积物中的Ga，Hf，In，Mo，Nb，Pb，Rb，Sn，Sr，Ta和Tl。该方法包括通过在压力分解铁氟龙容器中与HF + HNO_3 + HCl + H_3BO_3 + EDTA的混合物加热来溶解样品，然后使用感应耦合等离子体质谱（TCP / MS）直接定量测定。该方法比传统的通过开放式容器酸消解和融合以及通过仪器方法测定的样品溶解更快。通过对建立的痕量元素含量的许多国际地球化学参考样品进行重复分析，测试了所开发方法的准确性和精密度。发现与“推荐”或“共识”值具有令人满意的相关性，并且大多数情况下回收率为95-100％。本文首先报道了几种国际地球化学参考材料中Ga，In，Nb和Tl的新值。

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《Talanta: The International Journal of Pure and Applied Analytical Chemistry》 |1995年第12期|共11页
作者
J.G. Sen Gupta; N.B. Bertrand;
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正文语种 eng
中图分类分析化学;
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Geological materials; ICP-MS; Microwave decomposition; Multielement determination;

机译：地质材料ICP-MS微波分解多元素测定;

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1. Direct ICF-MS determination of trace and ultratrace elements in geological materials after decomposition in a microwave oven. Part II. Quantisation of Ba, Cs, Ga, Hf, In, Mo, Nb, Pb, Rb, Sn, Sr, Ta and T1 [J] . J.G. Sen Gupta, N.B. Bertrand Talanta: The International Journal of Pure and Applied Analytical Chemistry . 1995,第12期

机译：ICF-MS在微波炉中分解后直接测定地质材料中的痕量和超痕量元素。第二部分Ba，Cs，Ga，Hf，In，Mo，Nb，Pb，Rb，Sn，Sr，Ta和T1的量化
2. DIRECT DETERMINATION OF TRACES OF Ag, Cd, Pb, Bi, Cr, Mn, Co, Ni, Li, Be, Cu AND Sb IN ENVIRONMENTAL WATERS AND GEOLOGICAL MATERIALS BY SIMULTANEOUS MULTI-ELEMENT GRAPHITE FURNACE ATOMIC ABSORPTION SPECTROMETRY WITH ZEEMAN-EFFECT BACKGROUND CORRECTIO [J] . J.G. SEN GUPTA, J.L. BOUVIER Talanta: The International Journal of Pure and Applied Analytical Chemistry . 1995,第2期

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机译：一步一步微波辅助亚临界水萃取同时通过微波诱导等离子体光谱法测定参考材料中的无机元素（Ba，Ca，Cu，Fe，Mg，Mn，Na，Pb，Sr，Zn）
4. Program topic 6: Environmental Control Technologies for SOx, NOx, Particulets, and Trace Elements/Thermodynamics of Ttransition into a Gas Phase Hg, Cd, Zn, Pb, Se under Combustion and Gasification of Some Coals. [C] . Lebedeva L.N., Kost L.A., Gorlov E.G. International Pittsburgh Coal Conference . 2005

机译：程序主题6：用于在一些煤的燃烧和气化的气相Hg，Cd，Zn，Pb，Se中的SOx，NOx，术语和TTrannition的痕量元件/热力学的环境控制技术。
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机译：具有多个桥联配体的选定三钌簇中电子转移和氢活化的机理。第一部分。三氢三钌（亚烷基）簇中自由基反应性的减弱。通过歧化路径分解47电子簇自由基的电化学和动力学。第二部分通过（mu-hydrogen）（2）钌（3）（一氧化碳）（8）（mu-phosphorus（）的金属-金属键上氢的可逆氧化加成反应的动力学和机理激活过渡金属中心的分子氢t-BU）（2））（2）。
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7. Reviews: The Study of History: A Bibliographical Guide, the English Idea of History from Coleridge to Collingwood, the Changing Face of English Local History, Arthur and the English: The Arthurian Legend in Medieval English Life and Literature, Enacting Gender on the English Renaissance Stage, Shakespeare's Feminine Endings, Writing the English Republic: Poetry, Rhetoric and Politics 1627–1660, New Stories for Old: Biblical Patterns in the Novel, Catholicism and Anti-Catholicism in Early Modern English Texts, Primogeniture and Entail in England: A Survey of Their History and Representation in Literature, the English Civil War Through the Restoration in Fiction: An Annotated Bibliography, Diana, Self-Interest, and British National Identity, Dryden and the Traces of Classical Rome, between the Ancients and the Moderns: Baroque Culture in Restoration England, Bacchus in Romantic England: Writers and Drink, 1780–1830, Misogynous Economies: The Business of Literature in Eighteenth-Century Britain, the House of Forgery in Eighteenth-Century Britain, the Clothes That Wear Us, An Oxford Companion to the Romantic Age: British Culture, 1776–1832, Domestic Space: Reading the Nineteenth-Century Interior, Victorians in Theory: From Derrida to Browning, the Age of Virtue: British Culture from the Restoration to Romanticism, Woeful Afflictions: Disability and Sentimentality in Victorian America, Women Writers of the First World War: An Annotated Bibliography, the Pub in Literature, British Industrial Fictions, the Insatiability of Human Wants: Economics and Aesthetics in Market SocietyRichardsonR. C., The Study of History: A Bibliographical Guide , 2nd ed., Manchester University Press, 2000, pp. xiv + 140, £40.00.ParkerChristopher, The English Idea of History from Coleridge to Collingwood , Ashgate Publishing, 2000, pp. vii + 244, £45.RichardsonR. C. (ed.), The Changing Face of English Local History , Ashgate, 2000, pp. viii + 218, £45.00.BarronW. R. J. (ed.), Arthur and the English: The Arthurian Legend in Medieval English Life and Literature , University of Wales Press, 1999, pp. 398, £35.00.ComensoliViviana and RussellAnne (eds), Enacting Gender on the English Renaissance Stage , University of Illinois Press, 1999, pp. 270, £18.95; SaundersEve Rachel, Gender and Literacy on Stage in Early Modern England , Cambridge University Press, 1999, pp. 260, £35.BerryPhilippa, Shakespeare's Feminine Endings , Routledge, 1999, pp. 197, £15.99 pb.; BellIlona, Elizabethan Women and the Poetry of Courtship , Cambridge University Press, 1998, pp. 262, £35.00.NorbrookDavid, Writing the English Republic: Poetry, Rhetoric and Politics 1627–1660 , Cambridge University Press, 1999, pp. xiii + 509, £40.FischHarold, New Stories for Old: Biblical Patterns in the Novel , Macmillan, 1998, pp. x + 236, £42.50; FischHarold, The Biblical Presence in Shakespeare, Milton and Blake , Clarendon Press, 1999, pp. xi + 330, £45.MarottiArthur F. (ed.), Catholicism and Anti-Catholicism in Early Modern English Texts , Macmillan, 1999, pp. xvii + 266, £47.50; ShellAlison, Catholicism, Controversy and the English Literary Imagination, 1558–1660 , Cambridge University Press, 1999, pp. xi + 309, £37.50.JamoussiZouheir, Primogeniture and Entail in England: A Survey of their History and Representation in Literature , Centre de Publication Universitaire, Tunis, 1999, pp. 293, 8 DT.MurphRoxane C., The English Civil War through the Restoration in Fiction: An Annotated Bibliography , Greenwood Press, Westport, CT., 2000, pp. viii + 349, £63.95.HammondPaul, Dryden and the Traces of Classical Rome , Clarendon Press, Oxford, 1999, pp. 305, £45.00.LevineJoseph M., Between the Ancients and the Moderns: Baroque Culture in Restoration England , Yale University Press, 1999, pp. xiv + 279, £27.50.TaylorAnya, Bacchus in Romantic England: Writers and Drink, 1780–1830 , Macmillan, 1999, pp. xi + 264, £47.50.MandellLaura, Misogynous Economies: The Business of Literature in Eighteenth-century Britain , University of Kentucky, 1999, pp. x + 228, $42.00.BainesPaul, The House of Forgery in Eighteenth-century Britain , Ashgate, 1999, pp. viii + 195, £47.50.MunnsJessica and RichardsPenny (eds), The Clothes that Wear Us , Newark, University of Delaware Press, 1999, pp. 362, £37.McCalmanIain (ed.), An Oxford Companion to the Romantic Age: British Culture, 1776–1832 , Oxford University Press, 1999, p. xii + 780, £85.BrydenInga and FloydJanet (eds), Domestic Space: Reading the Nineteenth-century Interior , Manchester University Press, 1999, pp. xii + 219, £40.00; KiddAlan and NichollsDavid (eds), Gender, Civic Culture and Consumerism: Middle-class Identity in Britain 1800–1940 , Manchester University Press, 1999, pp. xiv + 223, £46.00, pb. £14.99.SchadJohn Victorians in Theory: From Derrida to Browning , Manchester University Press, 1999, pp. x + 180, £40.MorseDavid, The Age of Virtue: British Culture from the Restoration to Romanticism , Macmillan, 2000, pp. viii + 330, £45.KlagesMary, Woeful Afflictions: Disability and Sentimentality in Victorian America , University of Pennsylvania Press, 1999, pp. 211, $36.50.OudittSharon, Women Writers of the First World War: An Annotated Bibliography , Routledge, 2000, pp. 230, £75; TyleeClaire with TurnerElaine and CardinalAgnes (eds), War Plays by Women: An International Anthology , Routledge, 2000, pp. 225, £16.99 pb.TaylorJohn A., Diana, Self-Interest, and British National Identity , Praeger, 2000, pp. 169, £44.95.EarnshawSteven, The Pub in Literature , Manchester University Press, 2000, pp. x + 294, £45 and £15.99 pb.KlausH. 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机译：a-sITE-aND /或B-sITE-mODIFIED pBZRTIO3材料和（pB，sR，Ca，Ba，mG）（ZR，TI，NB，Ta）O3薄膜，具有铁电随机存取存储器和高性能薄膜微处理器的实用性

Direct ICF-MS determination of trace and ultratrace elements in geological materials after decomposition in a microwave oven. Part II. Quantisation of Ba, Cs, Ga, Hf, In, Mo, Nb, Pb, Rb, Sn, Sr, Ta and T1

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