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Video-controlled characterization of polymerization shrinkage in light-cured dental composites

机译:视频控制的光固化牙科复合材料中聚合收缩的表征

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This study investigated a procedure to measure the intrinsic polymerization contraction of dental resin-based materials. A CCD-camera interfaced with a computer through video-interface hardware measured the coordinates of the centers of gravity of two dot markers stuck on a resin composite cylinder before and after the irradiation. The distances of the centers of gravity, and hence the linear percentage shrinkage, were calculated. The values obtained were compared with those measured by the deflecting disk technique [D.C. Watts, A.J. Cash, Determination of polymerization shrinkage kinetics in visible-light-cured materials: methods development, Dent. Mater. 7 (1991) 281-287.], which assessed polymerization shrinkage through deflection of a glass disk measured by an linear vertical displacement transducer (LVDT). Three resin composites, light-cured for 40 s at 800 mW cm(-2), were tested: Solitaire 2 [SOL2], Tetric Ceram [TECE] and Z100 [Z100]. The data were subjected to the Kruskal-Wallis test (p < 0.05). Whatever the experimental procedure, the three resin composites did not present statistically different polymerization shrinkage, and data obtained with the video-controlled technique were statistically higher than with the deflecting disk method. (C) 2008 Elsevier Ltd. All rights reserved.
机译:这项研究调查了一种程序,以测量牙科树脂基材料的固有聚合收缩。通过视频接口硬件与计算机连接的CCD相机在辐照之前和之后测量粘贴在树脂复合材料圆柱体上的两个点标记的重心坐标。计算了重心的距离,从而计算出线性收缩百分比。将获得的值与通过偏转盘技术[D.C.瓦茨现金,可见光固化材料中聚合收缩动力学的测定:方法开发,Dent。母校参见,例如,J.Med.Chem.Soc.7(1991)281-287。],其通过由线性垂直位移传感器(LVDT)测量的玻璃盘的挠曲评估了聚合收缩率。测试了三种树脂复合材料,它们在800 mW cm(-2)下光固化40 s:纸牌2 [SOL2],Tetric Ceram [TECE]和Z100 [Z100]。数据经过Kruskal-Wallis检验(p <0.05)。无论采用哪种实验程序,这三种树脂复合材料在聚合收缩率上均没有统计学差异,并且通过视频控制技术获得的数据在统计学上高于偏转盘法。 (C)2008 Elsevier Ltd.保留所有权利。

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