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DESENVOLVIMENTO DE UM TITULADOR BASEADO NA CONTAGEM DE GOTAS

机译:计票支架的开发

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摘要

TitDrop II, a practice low-cost titrator based on drop counting is proposed. A microcomputer counts drops in an opto-switch and it receives pH values from a commercial pHmeter with RS-232 serial port. The volume of drops must kept constant and the amount of base in each drop is obtained by standardization in the titrator. A linear behavior between height of reservoir of titrant and drop frequency was observed, but there is no influence of low height on drop volume. Acetic acidity in samples of vinager was compared with volumetric titration, and deviation between -2.6 to 3.9% was observed.
机译:提出了TitDrop II,一种基于液滴计数的低成本低成本滴定仪。微型计算机计算光开关中的液滴,并从带有RS-232串行端口的商用pH计中接收pH值。滴液的体积必须保持恒定,并且每个滴液中的碱含量必须通过滴定仪中的标准化方法获得。观察到滴定剂的高度与液滴频率之间存在线性关系,但低高度对液滴体积没有影响。将醋酸乙烯酯样品中的醋酸与体积滴定法进行了比较,观察到的偏差在-2.6至3.9%之间。

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