Study of the Daughter Products of Akardite-II

摘要

In this work,five akardite-II (AK-II) daughter products were produced and isolated.Their respective MS,NMR,IR and UV spectra were recorded.These five products were positively identified as: N-NO-AK-II.2-NO_2-AK-II.4-NO_2-AK-II.N-NO-2-NO_2 AK-II and N-NO-4-NO_2-AK-II.An HPLC method giving baseline separation of 6 AK-II family products and 10 diphenyl-amine (DPA) family products is also described.Finally,preliminary results concerning the stability of AK-II daughter products are discussed.