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Novel Chitosan-TiO2 Nanohybrid: Preparation, Characterization, Antibacterial, and Photocatalytic Properties

机译:新型壳聚糖-TiO2纳米杂化物:制备,表征,抗菌和光催化性能。

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In this report, chitosan (CS) encapsulated titanium dioxide (TiO2) nanohybrid was prepared by chemical precipitation method. Fourier transform infrared spectroscopy (FT-IR) and X-ray diffraction (XRD) confirmed the formation of nanohybrid. Transmission electron microscopy (TEM) analysis showed the immobilization of TiO2 nanoparticles on the surface of CS. The nanohybrid was also characterized by thermogravimetric analysis (TGA) and zeta potential. The nanohybrid exhibited high photocatalytic activity as evident from the degradation of methylene blue (MB) dye. The result revealed substantial degradation of the MB dye (90%) under UV-light illumination. The catalytic efficiency was unaltered even after five cycles of reuse. In addition, the nanohybrid exhibited a superior antibacterial activity of 100% within 24 h of treatment against Escherichia coli (E. coli) was measured by colony forming units (CFU).
机译:在此报告中,壳聚糖(CS)封装的二氧化钛(TiO2)纳米杂化是通过化学沉淀法制备的。傅立叶变换红外光谱(FT-IR)和X射线衍射(XRD)证实了纳米杂化物的形成。透射电子显微镜(TEM)分析表明,TiO2纳米颗粒固定在CS表面。纳米杂化物还通过热重分析(TGA)和ζ电位进行表征。从亚甲基蓝(MB)染料的降解中可以明显看出,该纳米杂化物表现出高的光催化活性。结果表明,在紫外光照射下,MB染料(90%)显着降解。即使重复使用了五个循环,催化效率也没有改变。另外,通过菌落形成单位(CFU)测量,纳米杂交体在治疗的24小时内对大肠杆菌(E.coli)表现出100%的优异抗菌活性。

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