首页> 外文期刊>Journal of Nanostructures >Fabrication and Characterization of Zinc Sulfide Nanoparticles and Nanocomposites Prepared via a Simple Chemical Precipitation Method
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Fabrication and Characterization of Zinc Sulfide Nanoparticles and Nanocomposites Prepared via a Simple Chemical Precipitation Method

机译:通过简单的化学沉淀法制备的硫化锌纳米颗粒和纳米复合材料的表征

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In this research zinc sulfide (ZnS) nanoparticles and nanocomposites powders were prepared by chemical precipitation method using zinc acetate and various sulfur sources. The ZnS nanoparticles were characterized by X-ray diffraction, scanning electron microscopy, ultraviolet-visible and fourier transform infra-red. The structure of nanoparticles was studied using X-ray diffraction pattern. The crystallite size of ZnS nanoparticles was calculated by Debye–Scherrer formula. Morphology of nano-crystals was observed and investigated using the scanning electron microscopy. The grain size of zinc sulfide nanoparticles were in suitable agreement with the crystalline size calculated by X-ray diffraction results. The optical properties of particles were studied with ultraviolet-visible absorption spectrum.
机译:在这项研究中,硫化锌(ZnS)纳米颗粒和纳米复合材料粉末是通过使用乙酸锌和各种硫源的化学沉淀法制备的。 ZnS纳米粒子的特征在于X射线衍射,扫描电子显微镜,紫外可见光和傅立叶变换红外光谱。使用X射线衍射图谱研究了纳米颗粒的结构。 ZnS纳米粒子的微晶尺寸通过Debye–Scherrer公式计算。使用扫描电子显微镜观察并研究了纳米晶体的形态。硫化锌纳米粒子的晶粒尺寸与通过X射线衍射结果计算出的晶体尺寸适当吻合。用紫外可见吸收光谱研究了颗粒的光学性质。

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