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亚洲天然物产研究（英文版）

Journal of Asian Natural Products Research

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亚洲天然物产研究（英文版） >2001年第4期

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1.TRITERPENOID SAPONINS FROM THE LEAVES OF ILEX KUDINCHA
- MING-AN OUYANG;CHONG-REN YANG;ZHI-JUN WU;
- 《亚洲天然物产研究（英文版）》 | 2001年第1期
摘要：Eight new triterpenoid saponins, kudinosides I-P along with three known saponins were isolated from the leaves of Ilex kudincha. The aglycone moiety of kudinosides I-K was deter mined as a new triterpene (kudinolic acid), a fore-genin for the lactonic triterpene. The struc tures of all saponins were established on the basis of spectroscopic and chemical evidence. The biogenesis of the triterpene with lactonic moiety was briefly discussed.
2.ANDROECHIN, A NEW CHALCONE GLUCOSIDE FROM ANDROGRAPHIS ECHIOIDES
- B.JAYAPRAKASAM;D.GUNASEKAR;K.V.RAO;A.BLOND;B.BODO;
- 《亚洲天然物产研究（英文版）》 | 2001年第1期
摘要：A new chalcone glucoside, androechin, and a known flavone glucoside, echioidinin 5-O-gluco side, were isolated from the whole plant of Andrographis echioides. Androechin was character ized as 2,2',6'-trihydroxy-4'-methoxychalcone 2'-O-,β-D-glucopyranoside by spectral and chemical studies.
3.CHEMICAL CONSTITUENTS OF PSEUDOPTEROGORGIA SPECIES OF THE INDIAN OCEAN
- MULABAGAL VANISREE;GOTTUMUKKALA V.SUBBARAJU;CH.BHEEMASANKARA RAO;
- 《亚洲天然物产研究（英文版）》 | 2001年第1期
摘要：A new ceramide, (2S,3R,4E)-l,3-dihydroxy-2-[(hexadecanoyl)amino]-nonadeca-4-ene (1), chol est-5-en-3β,7β,19-triol (2), identified as its, peracetyl derivative (3), and batyl alcohol (4) were isolated from Pseudopterogorgia species. 1 exhibited antibacterial activity against Gram-positive and Gram-negative bacteria.
4.THREE NEW TRITERPENOIDS FROM FUSCOPORIA OBLIQUA
- JIAN HE;XIAO-ZHANG FENG;YANG LU;BIN ZHAO;
- 《亚洲天然物产研究（英文版）》 | 2001年第1期
摘要：Three new lanostane triterpenoids, fuscoporianol A (1), B (2), and C (3) were isolated from the petroleum ether extracts ofFuscoporia obliqua and their structures have been determined on the basis of chemical, spectroscopic methods and X-ray crystallographic analysis as 25-methoxy-21,22-cyclolanosta-8-ene-3β, 21a-diol (1), 3β; 22c-dihydroxy-lanosta-8, 23E-diene-25-peroxide (2),3β, 22a, 25-trihydroxy-lanosta-8, 23E-diene (3).
5.TWO NEW COMPOUNDS FROM PEUCEDANUM DECURSIVUM
- NIAN-HUAN YAO;LING-YI KONG;MASATAKE NIWA;
- 《亚洲天然物产研究（英文版）》 | 2001年第1期
摘要：Two new compounds, decuroside VI (1) and decursidate (2), were isolated from the roots of Peucedanum decursivum. Their structures were elucidated as 6'-O-crotonyl-nodakenin and 2-[4'-hydroxyphenyl]-glycol mono trans-ferulate on the basis of spectral analyses and chemi cal methods.
6.DIGLUCOSYLATION OF SALICYL ALCOHOL BY CELL SUSPENSION CULTURES OF SOLANUM LACINIATUM
- ACHMAD SYAHRANI;FRANSISCA HARTUTI;GUNAWAN INDRAYANTO;ALISTAIR L.WILKINS;
- 《亚洲天然物产研究（英文版）》 | 2001年第1期
摘要：A new biotransformation product, salicyl alcohol-7-O-β-D-(β-l,6-D-glucopyranosyl)-gluco pyranoside was isolated from cell suspension cultures of Solanum laciniatum, following administration of salicyl alcohol, and its structure was elucidated using a combination of one and two-dimensional 1H and 13C-NMR data, and positive and negative ion ESMS data.
7.CANCER CHEMOPREVENTIVE ACTIVITIES OF S-3-1,A SYNTHETIC DERIVATIVE OF DANSHINONE
- XIAO-GUANG CHEN;YAN LI;CHUN-HONG YAN;LIAN-NIANG LI;RUI HAN;
- 《亚洲天然物产研究（英文版）》 | 2001年第1期
摘要：Salvia miltiorrhiza is a traditional Chinese medicine which has been well documented for its anti-cancer effects. Based on the structure of danshinone, one of the active compounds derived from Salvia miltiorrhiza, we synthesized a simplified phenolic analog, S-3-1, and tried to explore its possible actions in preventing the development of cancer. With the Ames test, S-3-1 was found to efficiently suppress the mutagenicity of benzo[a]pyrene. This result is consistent with the inhibitory effect of S-3-1 on the activation of benzo[α]pyrene by hepatic microsomal enzymes. Besides the anti-initiation effects, S-3-1 could significantly inhibit the croton oil induced increase of mouse skin epithermal ornithine decarboxylase activity. Moreover, S-3-1 quenched both superoxide and hydroxyl free radicals whereas it inhibited lipid peroxidation in the in vitro model. These results suggest that S-3-1 might act as anti-initiation and anti-promo tion agents through reversing the biochemical alterations induced by carcinogen during carcino genesis. Therefore, we further investigated the effects of S-3-1 on carcinogenesis. In vitro, S-3-1inhibited the benzo[a]pyrene-induced transformation of V79 Chinese hamster lung fibroblasts.At 10-40 mg/kg, S-3-1 was found to inhibit the development of DM BA/croton oil-induced skin papilloma in mice through decreasing the incidence of papilloma, prolonging the latent period of tumor occurrence and reducing tumor number per mouse in a dose-dependent manner. We concluded from this study that S-3-1 might be developed as a new chemopreventive drug.
8.TWO NOVEL FLAVONOID GLYCOSIDES FROM CRATAEGUS PINNATIFIDA BGE.VAR. MAJOR N.E.BR.r
- PEI-CHENG ZHANG;YING-JUN ZHOU;SUI-XU XU;
- 《亚洲天然物产研究（英文版）》 | 2001年第1期
摘要：Two novel natural products, namely pinnatifida C, pinnatifida D, were isolated from the leaves of Crataegus pinnatifida Bge.var.rnajor N.E.Br. Their structures were elucidated by the spectro scopic analysis and chemical evidence.
9.FIVE NEW NORDITERPENOID ALKALOIDS FROM ACONITUM SINOMONTANUM
- FENG-PENG WANG;CHONG-SHENG PENG;XI-XIAN JIAN;DONG-LIN CHEN;
- 《亚洲天然物产研究（英文版）》 | 2001年第1期
摘要：From the roots of A conitum sinomontanum, five new norditerpenoid alkaloids, sinomontanitines A (1) and B (2), sinomontanines A (3), B (4) and C (5), were isolated together with the known alkaloids lappaconitine (6) and ranaconitine (7), The structures of the new alkaloids were determined by spectral analysis.
10.DITERPENOID ALKALOIDS FROM ACONITUM RACEMULOSUM FRANCH VAR. PENGZHOUENSE
- CHONG-SHENG PENG;XI-XIAN JIAN;FENG-PENG WANG;
- 《亚洲天然物产研究（英文版）》 | 2001年第1期
摘要：A new diterpenoid alkaloid, racemulotine (1), was isolated from the whole plants of Aconitum racemulosum Franch var. pengzhouense, and its structure was elucidated by 1D-and 2D-NMR spectra.
11.SAIKOSAPONIN v-1 FROM ROOTS OF BUPLEURUM CHINENSE DC.
- QIN-XIANG LIU;HONG LIANG;YU-YING ZHAO;BIN WANG;WEN-XIU YANG;YI YU;
- 《亚洲天然物产研究（英文版）》 | 2001年第2期
摘要：Three triterpenoidal saponins, saikosaponin v-l(1), 6″-O-acetyl-saikosaponin b2 (2) and 6"-O acetyl-saikosaponin d(3) were isolated from the roots of the title plant and the structures were identified on the basis of spectral analysis. Saikosaponin v-1 is a new compound, which was identified as 3β,16α,23,28-tetrahydroxy-olean-ll,13(18)-dien-30-oic acid-3-O-β-D-glucopyra nosyl-(1 → 3)-β-D-fucopyranosyl-30-O-xylitol ester.
12.TWO NEW GERMACRANOLIDES FROM MAGNOLIA GRANDIFLORA
- SHAO-HUA WU;XIAO-DONG LUO;YUN-BAO MA;XIAO-JIANG HAO;JUN ZHOU;DA-GANG WU;
- 《亚洲天然物产研究（英文版）》 | 2001年第2期
摘要：Two new sesquiterpenoids, 4,5-epoxy-13-methoxy-l(10)-germacren-12,6-olide and 4,5-epoxy 13-acetoxy-l(10)-germacren-12,6-olide, were isolated from the leaves of Magnolia grandiflora together with six known compounds, 2α-hydroxy-dihydroparthenolide, parthenolide, cos tunolide, syringaresinol, (+) medioresinol and 6,7-dimethoxycoumarin. The structures of the new compounds were elucidated on the basis of spectroscopic methods and X-ray diffraction.
13.NEW NORDITERPENOID ALKALOIDS FROM THE ROOTS OF ACONITUM GENICULATUM
- ZHENG-BANG LI;LIANG XU;XI-XIAN JIAN;FENG-PENG WANG;
- 《亚洲天然物产研究（英文版）》 | 2001年第2期
摘要：Four new norditerpenoid alkaloids, geniculatines A (1), B (4), C (7) and D (8), were isolated from the roots of Aconitum geniculatum Fletcher, and their structures were elucidated by spectral methods.
14.NEW 2-(2-PHENYLETHYL) CHROMONES FROM BOTHRIOCHLOA ISCHAEMUM
- TAO WANG;LAN-FANG LI;KUI ZHANG;WEN-YAN ZHANG;YUE-HU PEI;
- 《亚洲天然物产研究（英文版）》 | 2001年第2期
摘要：Two new 2-(2-Phenylethyl) chromones were isolated from Bothriochloa ischaemum (Grami neae). They were characterized as 5-hydroxy-6-methoxy-2-[2-(2-hydroxyphenyl)-ethyl]-chro mone(1) and 5-hydroxy-2-[2-(2-hydroxyphenyl)-ethyl]-chromone(2) by means of spectroscopic analysis, especially 2D-NMR experiments.
15.TRITERPENOID SAPONINS FROM LEAVES AND STEMS OF PANAX QUINQUEFOLIUM L.
- JIN-HUI WANG;WEN LI;YI SHA;YASUHIRO TEZUKA;SHIGETOSHI KADOTA;XIAN LI;
- 《亚洲天然物产研究（英文版）》 | 2001年第2期
摘要：In the chemical investigation on the saponin composition of leaves and stems of Panax quinquefolium L., two new minor dammarane saponins, quinquenoside L1 (1) and L2 (2) have been isolated. By means of physico-chemical evidences and spectral analysis their structures were established as 3-O-[β-D-glucopyranosyl-(1-2)-β-D-glucopyranosyl]-20-O-β-D-glucopyra nosyl-dammara-23,25-diene-3β, 12β, 20(S)-triol (1) and 3-O-[β-D-glucopyranosyl-(1-2)-β-D glucopyranosyl]-20-O-β-D-glucopyranosyl-(24Z)-dammar-24-ene-3β, 12β, 20(S), 26-tetraol (2).
16.TWO NOVEL PHENOLIC TRITERPENES FROM TRIPTERYGIUM WILFORDII
- GUANG-ZHONG YANG;MING-LEI XI;YUAN-CHAO LI;
- 《亚洲天然物产研究（英文版）》 | 2001年第2期
摘要：Two novel phenolic triterpenes were isolated from Tripterygium wilfordii Hook. f., their structures were identified to be 2,3-dihydroxy-1,3,5(10),8-tetra-ene-6α-(2′-hydroxyethyl)-24-nor-D:A-friedooleanane-29-oic acid 1, named triptotin F, and 2,3-dihydroxy-l,3,5(10),8-tetra ene-6β-(2'-hydroxyethyl)-24-nor-D:A-friedoo1eanane-29-oic acid 2, named triptotin G on the basis of spectroscopic studies.
17.CYTOCHALASIN D FROM HYPOCRELLA BAMBUSAE
- HONG XU;WEI-SHUO FANG;XIAO-GUANG CHEN;WEN-YI HE;KE-DI CHENG;
- 《亚洲天然物产研究（英文版）》 | 2001年第2期
摘要：Cytochalasin D which shows marked cytotoxic effects on multi-tumor cells was newly isolated at high content(5.28 mg/g, dry weight)from Fungus Hypocrella bambusae(B.et Br.) Sacc. Its structure was elucidated by spectroscopic methods. Two-dimensional NMR techniques were applied to make complete assignment for the 1H- and 13C-NMR chemical shifts of this compound.
18.PLATYPHYLLIN A, A NOVEL COUMARONE FROM THE LEAVES OF BETULA PLATYPHYLLA SUK.
- SU-JUAN WANG;YUE-HU PEI;HUI-MING HUA;
- 《亚洲天然物产研究（英文版）》 | 2001年第2期
摘要：A novel coumarone, platyphyllin A (1), was isolated from the leaves of Betula platyphylla Suk..The structure elucidation was accomplished by the analysis of spectroscopic data. Compound 1 was identified as a new coumarone skeleton, which was first isolated from plants.
19.CHESTNUTAMIDE: A NOVEL ALKALOID FROM FLOWERS OF CASTANEA MOLLISSIMA BLUME
- SI WANG;XING-BAO DING;YA-FEI CHEN;DE-QUAN YU;
- 《亚洲天然物产研究（英文版）》 | 2001年第2期
摘要：A novel alkaloid, chestnutamide, was isolated from the flowers of Castanea mollissima Blume.The structure was determined on the basis of spectral analysis.
20.STEREOSELECTIVE TOTAL SYNTHESIS OF CHRYSANTHEMOL
- LI-YUAN MOU;LI-YA ZHU;ZI-YUN LIN;XIA-OTIAN LIANG;
- 《亚洲天然物产研究（英文版）》 | 2001年第2期
摘要：Chrysanthemol (1), a trans-eudesmane type sesquiterpene from Chrysanthemum indicum L.,possesses certain anti-inflammatory activity. Its total synthesis was approached from two alternative routes and finally accomplished in ten steps from R-(+)-carvone via α-eudesmol (10) as the key intermediate. The overall yield is 2.4% and the spectral data of the synthetic target compound were identical with that of natural chrysanthemol (1). Seven intermediary compounds were tested for inhibitory effects on the carragenan-induced swelling of mouse paw but demonstrated no obvious activities.
21.C-27 AND C-3 GLUCOSYLATION OF DIOSGENIN BY CELL SUSPENSION CULTURES OF COSTUS SPECIOSUS
- GUNAWAN INDRAYANTO;SITI ZUMAROH;ACHMAD SYAHRANI;ALISTAIR L. WILKINS;
- 《亚洲天然物产研究（英文版）》 | 2001年第2期
摘要：3-O-[β-D-glucopyranosyl-(l″→ 2′)-β-D-glucopyranosyl], 27-O-β-D-glucopyranosyl-(25R)-spir ost-5-ene-3β,27-diol was isolated from cell suspension cultures of Costus speciosus, following incubation with diosgenin, and its structure was elucidated using a combination of one- and two-dimensional 1H and 13C NMR spectral data, and positive and negative ion ESMS spectral data.
22.SULFOGLYCOLIPID FROM THE MARINE BROWN ALGA SARGASSUM HEMIPHYLLUM
- ZHENG CUI;YU-SHAN LI;HONG-BING LIU;DAN YUAN;BAO-REN LU;
- 《亚洲天然物产研究（英文版）》 | 2001年第2期
摘要：One kinds of glycolipid (SBI) have been isolated from the marine brown alga Sargassum hemiphyllum (Turn.) Ag. The structures of SBI have been determined as the sodium salt of 1-0-acyl-3-0-(6′-sulfo-c-D-quinovopyrannosyl) glycerol (acyl: tetradecanoyl, pentadecanoyl, 11-hexadecenoyl, hexadecanoyl, 10,13-octadecadienoyl, 9-octade cenoyl, 15-metylheptadecanoyl and 11-eicosenoyl 17:1.5:19:153:1: 19:1:2) on the basis of chemical and spectral evidence and GC-MS analysis, respectively. Four constituents of the SBI were new compounds [the sodium salt of 1-0-(ll″-hexadecenoyl)-3-0-(6′-sulfo-α-D-quinovopyrannosyl) glycerol, the sodium salt of 1-0-(10",13"-octadecadienoyl)-3-0-(6′-sulfo-α-D-quinovopyrannosyl) glycerol,and the sodium salt of 1-0-(15"-metylhexadecenoyl)-3-0-(6′-sulfo-c-D-quinovopyrannosyl)glycerol, and the sodium salt of 1-0-(ll"-eicosenoyl)-3-0-(6′-sulfo-α-D-quinovopyrannosyl)glycerol]. All compounds were isolated from marine brown alga for the first time.
23.THE STRUCTURE OF PHYSALIN T FROM PHYSALIS ALKEKENGI VAR.FRANCHETI
- MASAO KAWAI;TATSUO YAMAMOTO;BUNSHO MAKINO;HATSUO YAMAMURA;SHUKI ARAKI;YASUO BUTSUGAN;KAZUKI SAITO;
- 《亚洲天然物产研究（英文版）》 | 2001年第3期
摘要：A new steroidal constituent named physalin T (3) was isolated from the aqueous extract of Physalis alkekengi var. francheti. Based on 1H and 13C NMR spectral studies the structure was assigned as 2,3-dihydrophysalin D, i.e., 5α,6β-dihydroxy-2,3,5,6-tetrahydrophysalin B, which is the first example of a natural physalin possessing a saturated ring A moiety. The structure was confirmed by the chemical transformation from the known physalin D (2) to physalin T.
24.A PAIR OF 24-HYDROPEROXYL EPIMERIC DAMMARANE SAPONINS FROM FLOWER-BUDS OF PANAX GINSENG
- FENG QIU;ZHONG-ZE MA;SUI-XU XU;XIN-SHENG YAO;CHUN-TAO CHE;YING-JIE CHEN;
- 《亚洲天然物产研究（英文版）》 | 2001年第3期
摘要：Further investigation on the saponins of the flower-buds of Panax ginseng C. A. Meyer has resulted in the isolation and structural elucidation of a pair of new 24-epimers of dammarane type saponins named ginsenoside I and II. The structures of the epimers were characterized on the basis of chemical and spectral evidence as 3-O-[β-D-glucopyranosyl-(1→2)-β-D-glucopyranosyl]-20-S-O-β-D-glucopyranosyl-3β,12β,20(S)-trihydroxy-24ξ-hydroperoxydam-mar-25-ene, except for their C-24 configurations. Ginsenoside Ⅰ is a new triterpene glycoside,and ginsenoside Ⅱ is a known compound first isolated from a natural plant.
25.ATEMOYACIN E, A BIS-TETRAHYDROFURAN ANNONACEOUS ACETOGENIN FROM ANNONA ATEMOYA SEEDS
- PING WU;WEN-SEN CHEN;TAI-SHAN HU;ZHU-JUN YAO;YU-LIN WU;
- 《亚洲天然物产研究（英文版）》 | 2001年第3期
摘要：Atemoyacin E (1), a new adjacent bis-tetrahydrofuran annonaceous acetogenin was isolated and characterized from the seeds of Annona atemoya.
26.TRITERPENE GLYCOSIDE FROM TERMINALIA ARJUNA
- R. K. UPADHYAY;M. B. PANDEY;R. N. JHA;V. P. SINGH;V. B. PANDEY;
- 《亚洲天然物产研究（英文版）》 | 2001年第3期
摘要：A new triterpene glycoside, arjunetoside, together with oleanolic and arjunic acids has been isolated from the root bark of Terminalia arjuna. The structure of arjunetoside has been established as 3-O-β-D-glucopyranosyl-2α,3β, 19α-trihydroxyolean-12-en-28-oic acid, 28-O-β-D-glucopyranoside by chemical and spectral data.
27.ECLALBATIN, A TRITERPENE SAPONIN FROM ECLIPTA ALBA
- R. K. UPADHYAY;M. B. PANDEY;R. N. JHA;V. B. PANDEY;
- 《亚洲天然物产研究（英文版）》 | 2001年第3期
摘要：From the whole plant of Eclipta alba, a new triterpene saponin, named eclalbatin, together with α-amyrin, ursolic acid and oleanolic acid were isolated. The structure of eclalbatin has been established as 3-0-β-D-glucopyranosyl-3-β-hydroxy-olean-12-en-28-oic acid, 28-0-β-D-arabino-pyranoside (1) on the basis of chemical and spectral data.
28.A NEW PHENOLIC GLYCOSIDE AND A NEW TRANS-CLERODANE DITERPENE FROM CONYZA BLINII
- YAN-FANG SU;DEAN GUO;YA-JUN CUI;JIAN-SHENG LIU;JUN-HUA ZHENG;
- 《亚洲天然物产研究（英文版）》 | 2001年第3期
摘要：A new phenolic glycoside, 4-propionyl-2,6-dimethoxyphenyl β-D-glucopyranoside (1) and a new trans-clerodane diterpene named 19-deacetylconyzalactone (2), were isolated from the aerial parts of Conyza blinii.
29.CHINESE BITTERSWEET ALKALOID Ⅲ,A NEW COMPOUND FROM CELASTR US ANGULATUS
- WEI-PING YIN;TIAN-ZENG ZHAO;JING-GUO FU;
- 《亚洲天然物产研究（英文版）》 | 2001年第3期
摘要：A novel skeleton alkaloid named Chinese Bittersweet Alkaloid Ⅲ from the leaves of C. angulatus was reported. The structure and its stereochemistry were established by IR, 1Dand 2DNMR (1H-1HCOSY, HMQC, HMBC, NOESY), MS and elemental analysis.
30.SESQUITERPENE GLUCOSIDES FROM ANTI-LEUKOTRIENE B4 RELEASE FRACTION OF TARAXACUM OFFICINALE
- YOSHIKI KASHIWADA;KOICHIRO TAKANAKA;HARUMI TSUKADA;YOSHIHISA MIWA;TORU TAGA;SHIGEO TANAKA;YASUMASA IKESHIRO;
- 《亚洲天然物产研究（英文版）》 | 2001年第3期
摘要：Chemical examination of the MeOH extract of the root of Taraxacum officinale, which exhibited inhibitory activity on the formation of leukotriene B4 from activated human neutrophils, has resulted in the isolation of 14-O-β-D-glucosyl-11,13-dihydro-taraxinic acid (1)and 14-O-β-D-glucosyl-taraxinic acid (2). The absolute stereostructure of 1 has been established by X-ray chrystallographic examination.

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