High-temperatire Calorimetry of Fusion Reactor Blanket Materials

摘要

The experimental techniques of high-temperature heat flow calorimetry are explained in view of selection and mass optimisation of standards for caloric calibration, condition of samples, heating rates and liner materials, Calorimetric work is illustrated on enthalpy measurements of Li_4SiO_4, Li_2SiO_3, Li_2ZrO_3, LiAlO_2 and Li_2TiO_3 by isothermal drop calorimetry and by heat capacity calculations therefrom.