X-ray powder diffraction data for two new N-substituted 3,4-dihydrospiro-2(1H) quinolines

摘要

The X-ray powder diffraction patterns for two N-substituted tetrahydroquinolines are report- ed. N-(α-Chloroacetyl)-6-methoxy-3,4-dihydro-4-methylspiro[cyclohexane-1, 2(1H) quinoline], C_18H_24CINO_2, and N-(α-chloroacetyl)-6-methoxy-3, 4-dihydro-4-methylspiro[cyclohexane-1, 2(1H)- Quinoline], C_17H_21Cl_2No are monoclinic, with refined unit cell parameters a=1.4471(3), b =0.9600(4), C=1.1948(3) nm, β=93.21(2)~0, V=1.6573(6) nm~3, Z=4, D_x=1.29 g cm~-3, and a=1.4487(3), b=0.9878(2), c=1.1390(2) nm, β=91.66(2), v=1.6294(4) nm~3, z=4, and D_x=1.32g cm~-3, respectively, with space group p2_1 (NO.14).