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Quantitative phase analysis of natural products using whole-powder-pattern decomposition

机译:利用全粉模式分解对天然产物进行定量相分析

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摘要

The capability of whole-powder-pattern decomposition in the quantitative phase analysis (QPA) of natural products was investigated using three- to six-component mixtures and pottery bodies. Here, the term pottery body means plastic clay suitable for making pottery and it is compounded of ceramic raw materials. Average errors of the weight fractions for each phase were within 1 weight percent in each mixture of natural products. The amounts of reduced oxides in pottery bodies derived from the X-ray diffraction technique were in good agreement with results obtained by X-ray fluorescence analysis. The present procedure does not require knowledge of crystal structures; it appears adequate for the QPA of natural products.
机译:使用三至六组分混合物和陶体,研究了天然产物定量相分析(QPA)中全粉体模式分解的能力。在此,术语“陶体”是指适用于制造陶器的塑料粘土,它是由陶瓷原料制成的。在天然产物的每种混合物中,每个相的重量分数的平均误差在1重量百分比以内。由X射线衍射技术得出的陶瓷体中还原氧化物的含量与通过X射线荧光分析获得的结果非常吻合。本程序不需要晶体结构的知识。它似乎足以满足天然产品的QPA。

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