X-ray powder diffraction analysis of a silver(I)-aspartame complex

R. Putvinskis; C. O. Paiva-Santos; M. Cavicchioli; A. C. Massabni

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X-ray powder diffraction analysis of a silver(I)-aspartame complex

机译：银（I）-阿斯巴甜络合物的X射线粉末衍射分析

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Synchrotron X-ray powder diffraction (XRPD) data were collected for the silver(I)-aspartame complex [Ag(C_(14)H_(17)N_2O_5)]·1/2 H_2O. The complex was obtained from a stoichiometric mixture of aspartame (3-amino-N-(α-carboxyphenethyl)-succinamic acid N-methyl ester, C_(14)H_(18)N_2O_5), Na_2CO_3, and AgNO_3. Indexing using Crysfire and Chekcell proposed an orthorhombic unit cell with space group P222_1. The lattice parameters are a= 12.4750(1) A, b=21.60614(14) A, and c =4.88888(9) A.

机译：收集银（I）-阿斯巴甜络合物[Ag（C_（14）H_（17）N_2O_5）]·1/2 H_2O的同步加速器X射线粉末衍射（XRPD）数据。该复合物是从阿斯巴甜（3-氨基-N-（α-羧基苯乙基）-琥珀酸N-甲酯，C_（14）H_（18）N_2O_5），Na_2CO_3和AgNO_3的化学计量混合物中获得的。使用Crysfire和Chekcell进行索引提出了空间群为P222_1的正交晶胞。晶格参数为a = 12.4750（1）A，b = 21.60614（14）A和c = 4.88888（9）A.

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来源
《Powder diffraction》 |2006年第4期|p.314-317|共4页
作者
R. Putvinskis; C. O. Paiva-Santos; M. Cavicchioli; A. C. Massabni;
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作者单位

Laboratorio Computacional de Analises Cristalograficas e Cristalinas -LabCACC, Instituto de Quimica, UNESP, 14800-900, Rua Prof. Francisco Degni s, Araraquara, SP, Brazil;

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收录信息美国《科学引文索引》(SCI);美国《生物学医学文摘》(MEDLINE);
原文格式 PDF
正文语种 eng
中图分类工程材料学;
关键词
silver(I)-aspartame; X-ray diffraction; le bail method;

机译：银（I）-阿斯巴甜;X射线衍射;保释法;

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X-ray powder diffraction analysis of a silver(I)-aspartame complex

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