Synthesis and X-ray diffraction data of dichlorodioxido (4,4-dimethoxycarbonyl-2,2′-bipyridyl) molybdenum(Ⅵ)

H.A. Camargo; N.J. Castellanos; C.C. Rosas; J.A. Henao

首页> 外文期刊>Powder diffraction >Synthesis and X-ray diffraction data of dichlorodioxido (4,4-dimethoxycarbonyl-2,2′-bipyridyl) molybdenum(Ⅵ)

【24h】

Synthesis and X-ray diffraction data of dichlorodioxido (4,4-dimethoxycarbonyl-2,2′-bipyridyl) molybdenum(Ⅵ)

机译：二氯二氧化物（4,4-二甲氧基羰基-2,2'-联吡啶基）钼（Ⅵ）的合成及X射线衍射数据

获取原文

获取原文并翻译 | 示例

掌桥外文数据库（机构版） >>

开具论文收录证明 >>

页面导航

摘要
著录项
相似文献
相关主题

摘要

The dichlorodioxido(4,4′-dimethoxycarbony1-2,2′-bipyridyl)molybdenum(Ⅵ) complex was prepared from molybdenum(Ⅵ) dichloride dioxide and 4,4-dimethoxycarbony1-2,2-bipyridyl in CH_2Cl_2 obtaining a clear green solution. The molybdenum complex was separated by precipitation with ethyl ether. The XRPD pattern for the new compound showed that the crystalline compound belongs to the monoclinic space group P2_1/c (No 14) with refined unit-cell parameters a = 12.104(1) A, b = 14.933 (2) A, c = 11.010 (2) A and β = 115.409° (9). The volume of the unit cell is V= 1797.6 (3) A~3.

机译：由二氯化钼（Ⅵ）和4,4-二甲氧基羰基1-2,2-联吡啶在CH_2Cl_2中制得二氯二氧化物（4,4'-二甲氧基碳酸1-2,2'-联吡啶基）钼（Ⅵ），得到透明的绿色溶液。。通过用乙醚沉淀分离钼配合物。新化合物的XRPD图谱显示该结晶化合物属于单斜晶空间群P2_1 / c（No 14），其精炼的晶胞参数a = 12.104（1）A，b = 14.933（2）A，c = 11.010 （2）A和β= 115.409°（9）。晶胞的体积为V = 1797.6（3）A〜3。

著录项

来源
《Powder diffraction》 |2014年第1期|42-45|共4页
作者
H.A. Camargo; N.J. Castellanos; C.C. Rosas; J.A. Henao;
展开▼
作者单位

Grupo de Investigation en Nuevos Materiales y Energias Alternativas (GINMEA), Facultad de Quimica Ambiental,Universidad Santo Tomds, Campus Universitario Floridablanca, Santander, Colombia;

Grupo de Investigation en Nuevos Materiales y Energias Alternativas (GINMEA), Facultad de Quimica Ambiental,Universidad Santo Tomds, Campus Universitario Floridablanca, Santander, Colombia;

Grupo de Investigation en Nuevos Materiales y Energias Alternativas (GINMEA), Facultad de Quimica Ambiental,Universidad Santo Tomds, Campus Universitario Floridablanca, Santander, Colombia;

Grupo de Investigation en Quimica Estructural (GIQUE). Escuela de Quimica, Facultad de Ciencias,Universidad Industrial de Santander, A.A. 678, Carrera 27, Calle 9 Ciudadela Universitaria, Bucaramanga, Colombia;

展开▼
收录信息美国《科学引文索引》(SCI);美国《生物学医学文摘》(MEDLINE);
原文格式 PDF
正文语种 eng
中图分类
关键词
dioxomolybdenum complex; X-ray powder diffraction; biomimetic compounds;

机译：二氧钼复合物;X射线粉末衍射;仿生化合物;
入库时间 2022-08-17 13:09:31

相似文献

外文文献
中文文献
专利

1. Synthesis, spectral and cyclic voltammetric studies on (4,4 '-bipyridyl)bis(di(2-hydroxyethyl)dithiocarbamato)zinc(II) and (4,4 '-bipyridyl)bis(bis(N-methyl, N-ethanoldithiocarbamato)zinc(II) and their X-ray crystal structures [J] . Manohar A., Bocelli G., Righi L., Inorganica Chimica Acta . 2001,第1a2期

机译：（4,4'-联吡啶基）双（二（2-羟乙基）二硫代氨基甲酸酯）锌（II）和（4,4'-联吡啶基）双（双（N-甲基，N-乙醇二硫代氨基甲酸酯）的合成，光谱和循环伏安研究锌（II）及其X射线晶体结构
2. Synthesis, spectral and cyclic volmtammetric studies on (4,4'-bipyridyl)bis(di(2-hydroxyethyl)dithiocarbamato)zinc(II) and (4,4'-bipyridyl)bis(bis(N-methyl, N-ethanoldithiocarbamato)zinc(II) and their X-ray crystal structures [J] . Arumugam Manohar, Kuppukkannu Ramaligam, Gabriele Bocelli, Inorganica Chimica Acta . 2001,第1a2期

机译：（4,4'-联吡啶）双（二（2-羟乙基）二硫代氨基甲酸酯）锌（II）和（4,4'-联吡啶基）双（双（N-甲基，N-乙醇二硫代氨基甲酸酯）的合成，光谱和循环伏安研究锌（II）及其X射线晶体结构
3. Biomimetic synthesis of 4,4'-dimethoxycarbonyl-2,2'-bioxazole [J] . Wieslaw Z.Antkowiak, Izabella Kopysc-Lapinska Heterocycles: An International Journal for Reviews and Communications in Heterocyclic Chemistry . 2003,第1期

机译：仿生合成4,4'-二甲氧基羰基-2,2'-生物恶唑
4. Synthesis And Powder X-ray Diffraction Studies On Copper(II) Complexes Of 4,4'-Diaminodiphenyl Sulfone [C] . L. Jaideva Singh, R.K. Hemakumar Singh, R. Chitra, DAE Solid State Physics Symposium . 2011

机译：4,4'-二氨基二苯基砜的铜（II）复合物的合成和粉末X射线衍射研究
5. Synthesis and characterization of novel platinum(II) and platinum(IV) complexes containing 4,4'-disubstituted-2,2'- bipyridine ligands for the treatment of cancer. [D] . Vo, Van. 2014

机译：含有4,4'-双取代-2,2'-联吡啶配体的新型铂（II）和铂（IV）配合物的合成和表征，用于治疗癌症。
6. Synthesis, characterization, and debromination reactivity of cellulose-stabilized Pd/Fe nanoparticles for 2,2',4,4'-tretrabromodiphenyl ether [O] . Guofu Huang, Mianmian Wang, Yongyou Hu, 2012

机译：纤维素稳定的Pd / Fe纳米粒子对2,2'，4,4'-四溴二苯醚的合成，表征和脱溴反应性
7. Synthesis and Characterization of Some Metal Complexes with their Sulfamethoxazoleand 4,4'-dimethyl-2,2'-bipyridyl and study Cytotoxic Effect on Hep-2 Cell Line [O] . Baghdad Science Journal 2015

机译：用磺胺甲恶唑的4,4'-二甲基-2,2'-双吡啶基合成与表征一些金属配合物对Hep-2细胞系的细胞毒性作用
8. SYNTHESIS OF DIFLUORAMINOHEXANITROBIPHENYL COMPOUNDS:3-DIFLUORAMINO-2,2',4,4',6,6'-HEXANITROBIPHENYL AND 3,3'-BIS(DIFLUORAMINO)-2,2',4,4',6,6'-HEXANITROBIPHENYL [R] . Michael W. Lerom, Howard M. Peters, Donald L. Ross 1972

机译：二氟氨基甲烷基苯基化合物的合成：3-二氟氨基-2,2'，4,4'，6,6'-六硝基苯基和3,3'-BIs（二氟氨基）-2,2'，4,4'，6,6' -HEXaNITROBIpHENYL

Synthesis and X-ray diffraction data of dichlorodioxido (4,4-dimethoxycarbonyl-2,2′-bipyridyl) molybdenum(Ⅵ)

摘要

著录项

相似文献

相关主题

期刊订阅