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Characterization of perovskite film prepared by pulsed laser deposition on ferritic stainless steel using microscopic and optical methods

机译:用显微和光学方法表征脉冲激光沉积在铁素体不锈钢上制备的钙钛矿薄膜

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摘要

The perovskite La0.6Sr0.4Co0.2Fe0.8O3-delta (LSCF48) film was deposited on Crofer 22 APU ferritic stainless steel by pulsed laser deposition (PLD). Morphological studies of the sample were performed using scanning electron microscopy (SEM) and atomic force microscopy (AFM). Information about film thickness and surface topography of the film and the steel substrate were obtained using following optical methods: spectroscopic ellipsometry (SE), bidirectional reflection distribution function (BRDF) and total integrated reflectometry (TIS). In particular, the BRDF study, being complementary to atomic force microscopy, yielded information about surface topography. Using the previously mentioned methods, the following statistic surface parameters were determined: root-mean square (rms) roughness and auto correlation length by determining the power spectral density (PSD) function of surface irregularities. (C) 2015 Elsevier B.V. All rights reserved.
机译:通过脉冲激光沉积(PLD)将钙钛矿型La0.6Sr0.4Co0.2Fe0.8O3-δ(LSCF48)膜沉积在Crofer 22 APU铁素体不锈钢上。使用扫描电子显微镜(SEM)和原子力显微镜(AFM)对样品进行形态学研究。使用以下光学方法获得有关膜和钢基材的膜厚度和表面形貌的信息:光谱椭圆仪(SE),双向反射分布函数(BRDF)和全积分反射仪(TIS)。特别是,BRDF研究作为原子力显微镜的补充,提供了有关表面形貌的信息。使用前面提到的方法,确定了以下统计表面参数:通过确定表面不规则性的功率谱密度(PSD)函数,确定了均方根(rms)粗糙度和自相关长度。 (C)2015 Elsevier B.V.保留所有权利。

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