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Effect of liquid medium temperature on the production rate and quality of graphene nanosheets produced by laser ablation

机译:液体介质温度对激光烧蚀石墨烯纳米片生产速率和质量的影响

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摘要

Effect of the liquid medium temperature on the characteristics of carbon nanostructures produced by pulsed laser ablation process in distilled water is investigated experimentally. The fundamental wavelength of a Q-switched Nd:YAG laser was employed to irradiate a high purity graphite target in distilled water at different temperatures of 0, 20, 35, 50 and 65 ℃. Produced carbon nanostructures were diagnosed by UV-Vis-NIR spectroscopy, FTIR spectrum, X-ray diffraction pattern, transmission electron microscopy, field emission scanning electron microscopy, dynamic light scattering and Raman scattering spectrum. Results show that graphene nanosheets and carbon nanopar-ticles were produced in all temperatures. With increasing the temperature of ablation liquid the number of carbon nanoparticles increases while the rate of graphene nanosheets production decreases.
机译:实验研究了液体介质温度对脉冲激光烧蚀过程在蒸馏水中产生的碳纳米结构特征的影响。采用Q开关Nd:YAG激光的基波波长在0、20、35、50和65℃不同温度下在蒸馏水中辐照高纯度石墨靶。通过UV-Vis-NIR光谱,FTIR光谱,X射线衍射图,透射电子显微镜,场发射扫描电子显微镜,动态光散射和拉曼散射光谱来诊断产生的碳纳米结构。结果表明,在所有温度下均产生了石墨烯纳米片和碳纳米粒子。随着烧蚀液温度的升高,碳纳米颗粒的数量增加,而石墨烯纳米片的生产率降低。

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