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Effect of Trace Element Hf on the Precipitation Process and Recrystallization Resistance of Al-Er-Zr Alloys

机译:微量元素Hf对Al-Er-Zr合金沉淀过程和抗再结晶性的影响

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摘要

Vickers hardness and electric conductivity measurements as well as micro-structure analysis were used to investigate the effects of trace element Hf atoms on the precipitation and recrystallization resistance in Al-Er-Zr alloys. The results of the present study indicated that the behaviors of precipitation process in Al-0.04Er-0.08Zr and Al-0.04Er-0.08Zr-0.05Hf (at. %) alloys are similar. When alloys were annealed at 350 ℃ for 96h, the nano-scale and coherent Al_3(Er, Zr) and Al_3(Er, Zr, Hf) precipitates form, corresponding to the peak hardness values of 56.2 ± 0.9 (ternary alloy), 58.9 ±1.5 HV (quaternary alloy), respectively. The higher peak hardness in Al-0.04Er-0.08Zr-0.05Hf alloys mainly benefit from the decomposition of Hf. It was shown that the existence of precipitates could improve the recrystallization resistance obviously. Due to the similar retarding force, recrystallization temperatures of both alloys are almost the same, approximate 450 ℃.
机译:使用维氏硬度和电导率测量以及微观结构分析来研究痕量元素Hf原子对Al-Er-Zr合金的析出和抗再结晶性的影响。本研究结果表明,Al-0.04Er-0.08Zr和Al-0.04Er-0.08Zr-0.05Hf(原子%)合金中的析出过程行为相似。当合金在350℃退火96h时,会形成纳米级连贯的Al_3(Er,Zr)和Al_3(Er,Zr,Hf)析出,对应于56.2±0.9(三元合金)的峰值硬度值58.9。分别为±1.5 HV(四元合金)。 Al-0.04Er-0.08Zr-0.05Hf合金中较高的峰值硬度主要受益于Hf的分解。结果表明,析出物的存在可以明显提高抗再结晶性。由于相似的阻滞力,两种合金的再结晶温度几乎相同,约为450℃。

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