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Synthesis and Characterization of Strontium Oxide Nanoparticles via Wet Process

机译:湿法合成氧化锶纳米粒子及其表征

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Strontium Oxide (SrO) nanopowder was synthesized by hydrolysis of single source molecular precursor SrCl_2 • 6H_2O with potassium hydroxide. The structure, morphology and properties of the particle were characterized by XRD, TEM, Raman and UV-vis-spectroscopy. The mean particle size (28.6 nm) was calculated by using X-ray diffraction pattern. A crystalline nature and with controlled particle distribution and phase purity was established with XRD and FT-IR. The crystallite size and phase purity increases with temperature which depends on the molar ratio of the starting molecular precursor, pH, temperature, reaction time along with its synthetic methodology.
机译:通过用氢氧化钾水解单源分子前驱体SrCl_2•6H_2O合成了氧化锶(SrO)纳米粉。通过XRD,TEM,拉曼和紫外可见光谱对颗粒的结构,形态和性能进行了表征。通过使用X射线衍射图计算平均粒径(28.6nm)。用XRD和FT-IR确定了晶体性质,并具有受控的颗粒分布和相纯度。微晶尺寸和相纯度随温度而增加,这取决于起始分子前体的摩尔比,pH,温度,反应时间及其合成方法。

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