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首页> 外文期刊>Materials Focus >Rapid Sonochemically Assisted and Environmentally Benign Green Synthesis of Silver Iodide Nanoparticles with Photocatalytic Properties
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Rapid Sonochemically Assisted and Environmentally Benign Green Synthesis of Silver Iodide Nanoparticles with Photocatalytic Properties

机译:快乐型辅助和环境良性绿化合成光催化性能的碘化银纳米粒子

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摘要

The aim of the present work was to explore the effect of D-glucose as reducing agent as well as capping agent in the ultrasound wave mediated sonochemical synthesis of AgI nanoparticles. In the present research work, spherical shaped AgI nanoparticles (NPs) are produced by using a mixtureof silver nitrates, potassium iodide as precursors and D-glucose as reducing agent. The eco-friendly synthesized silver iodide NPs were characterized by powder X-ray diffraction (PXRD), scanning electron microscopy (SEM), energy dispersive X-ray spectroscopy (EDX), Fourier transform infraredspectroscopy (FTIR), UV-Vis spectroscopy and photoluminescence (PL) spectroscopy. The PXRD result indicates crystalline nature of AgI NPs with the particle size of 27 ± 3 nm respectively. In addition, the photocatalytic degradation of the AgI NPs was evaluated by the decomposition oforganic dyes with a concentration of 10 ppm under visible light irradiation. The highlights of utilizing D-glucose in sonochemical synthesis of AgI NPs is less reaction time, economic, eco-friendly, one step method and is devoid of organic solvents which are toxic to living organisms as wellas the environment.
机译:本作本作的目的是探讨D-葡萄糖作为还原剂的效果以及超声波介导的AGI纳米颗粒的超声波合成中的封端剂。在本研究工作中,通过使用硝酸银,碘化钾作为前体和D-葡萄糖作为还原剂来制备球形AGI纳米颗粒(NPS)。 ECO友好的合成银碘化银NPS以粉末X射线衍射(PXRD),扫描电子显微镜(SEM),能量分散X射线光谱(EDX),傅里叶变换红外光谱(FTIR),UV-Vis光谱和光致发光(PL)光谱学。 PXRD结果表明AGI NP的结晶性质分别具有27±3nm的粒度。此外,通过在可见光照射下的浓度为10ppm的浓度的染料分解评估AGI NP的光催化降解。利用D-葡萄糖在Sonocheochemical合成的亮点较少反应时间,经济,环保,一步法较少,缺乏有机溶剂,这些有机溶剂对生物体毒性有毒。

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