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Influence of La_2O_3 nanoparticle additions on microstructure, wetting, and tensile characteristics of Sn-Ag-Cu alloy

机译:La_2O_3纳米粒子的添加对Sn-Ag-Cu合金的组织,润湿和拉伸特性的影响

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摘要

In this study, the effect of La_2O_3 nanoparticles (0, 0.01, 0.03, 0.05 and 0.1 wt.%) has been investigated in Sn-3.0Ag-0.5Cu (SAC-305) alloy. The various soldering properties have been tested, such as wettability, microstructural evolution, intermetallic compound formation, micro-hardness, tensile strength, and fracture analysis of tensile tested samples. La_2O_3 nanoparticles are added in the Sn-3.0Ag-0.5Cu alloy by mechanical mixing of powders and melting. The structural and morphological features of the samples are characterized by X-ray diffraction (XRD), scanning electron microscope (SEM), and electron probe micro-analyzer (EPMA). The experimental results indicate that the best combination of microstructural, wetting and tensile properties is obtained at 0.05 wt.% La_2O_3 in the solder matrix. The sample reinforced with 0.05 wt.% La_2O_3 i.e., SAC-0.05 La2O3 exhibits ~18% increase in microhardness, ~26% increase in the ultimate tensile strength (UTS), and ~14% elongation due to the adsorption of high surface energy of La_2O_3 nanoparticles in the matrix.
机译:在这项研究中,已经研究了La_2O_3纳米粒子(0、0.01、0.03、0.05和0.1 wt。%)在Sn-3.0Ag-0.5Cu(SAC-305)合金中的作用。已测试了各种焊接性能,例如润湿性,微观结构演变,金属间化合物形成,显微硬度,拉伸强度以及拉伸测试样品的断裂分析。通过粉末的机械混合和熔化将La_2O_3纳米颗粒添加到Sn-3.0Ag-0.5Cu合金中。样品的结构和形态特征通过X射线衍射(XRD),扫描电子显微镜(SEM)和电子探针显微分析仪(EPMA)进行表征。实验结果表明,在焊料基体中以0.05 wt。%La_2O_3获得了微观结构,润湿性和拉伸性能的最佳组合。用0.05 wt。%La_2O_3增强的样品,即SAC-0.05 La2O3,由于其高表面能的吸附,其显微硬度提高了约18%,极限抗拉强度(UTS)增长了约26%,伸长率达到了14%。基质中的La_2O_3纳米粒子。

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