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Preparation of Zirconia-toughened Alumina Ceramics through the Dispersal Basic Carbonate Precursors

机译:分散碱式碳酸盐前驱体制备氧化锆增韧氧化铝陶瓷

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摘要

Using NH_4HCO_3 solution as precipitant, the ultrafine 3Y-ZrO_2/Al_2O_3 precursors were prepared by the liquid-phase precipitation method. The well-dispersible ZrO_2/Al_2O_3 composite nanopowders with particle size 10nm were obtained by calcining the precursor at 1000℃. The XRD patterns show no γ-Al_2O_3 and θ-Al_2O_3 formed during calcination. The powders have excellent sinterability and the relative density of specimen is up to 99% after sintering the green compacts at 1550℃. Microstructural analysis of the sintered bodies reveals the uniform distribution of the zirconia grains in the alumina matrix.
机译:以NH_4HCO_3溶液为沉淀剂,通过液相沉淀法制备了超细的3Y-ZrO_2 / Al_2O_3前驱体。将前驱体在1000℃下煅烧,得到分散性好的ZrO_2 / Al_2O_3复合纳米粉。 XRD图谱显示在煅烧过程中没有形成γ-Al_2O_3和θ-Al_2O_3。该粉末具有良好的烧结性,在1550℃下烧结生坯后,样品的相对密度高达99%。烧结体的微观结构分析表明,氧化锆晶粒在氧化铝基体中的分布均匀。

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