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Investigations on physical properties of Mg ferrite nanoparticles for microwave applications

机译:微波应用镁铁氧体纳米粒子的物理性能研究

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Nanocrystalline Mg-ferrites have been synthesized by sol-gel auto combustion method using citric acid as fuel agent at different Calcination temperatures (200 degrees C, 400 degrees C, 600 degrees C, and 800 degrees C). The physical properties of nano Mg-ferrite were investigated using X-ray diffraction (XRD) analysis, scanning electron microscopy, Fourier-transform infrared spectroscopy, and LCR-Hitester for structural, surface morphology, functional groups and dielectric properties respectively. The single-phase cubic spinel structure of all the samples has been confirmed by XRD. Surface morphology studies reveal that the grains are clear with well-defined grain boundaries and also found that the average grain size is maximum at 600 degrees C calcination temperature. The dielectric studies reveal that the maximum dielectric constant is attained a value of 46 with the minimum dielectric loss at 600 degrees C calcination temperature.
机译:通过使用柠檬酸作为燃料在不同的煅烧温度(200摄氏度,400摄氏度,600摄氏度和800摄氏度)下通过溶胶-凝胶自动燃烧法合成了纳米晶Mg铁氧体。利用X射线衍射(XRD)分析,扫描电子显微镜,傅立叶变换红外光谱和LCR-Hitester研究了纳米镁铁氧体的物理性质,分别用于结构,表面形态,官能团和介电性质。 XRD证实了所有样品的单相立方尖晶石结构。表面形态研究表明,晶粒清晰,边界清晰,并且在600℃的煅烧温度下平均晶粒尺寸最大。介电研究表明,在600摄氏度的煅烧温度下,最大介电常数达到46,最小介电损耗。

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