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Structural, optical and luminescence properties of pure, Fe-doped and glucose-capped CdO Semiconductor nanoparticles for their Antibacterial activity

机译:纯,Fe掺杂和葡萄糖封端CDO半导体纳米粒子的结构,光学和发光性能,用于其抗菌活性

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摘要

Single-phase pure, Fe-doped and glucose-capped CdO nanoparticles (NPs) were prepared by a chemical precipitation method. The structure, morphology, composition, optical and luminescence properties of all samples were investigated using X-ray powder diffraction (XRD), scanning electron microscopy (SEM), Fourier transform infrared (FTIR) spectroscopy, photoluminescence (PL), and ultraviolet-visible (UV-Vis) spectroscopy. XRD study revealed the single-phase hexagonal crystal structure of all samples with P63/mmc space group. SEM detected the microstructural behaviour of all samples. The functional groups of the synthesized samples were also identified by FTIR spectroscopy. The calculated direct band energy values were estimated as 3.78 eV for pure, 3.65 eV for Fe-doped, and 3.63 eV for glucose-capped CdO NPs. From PL study, it was identified that glucose-capped CdO NPs showed the strongest photoluminescence signal (543 nm) comparing to the Fe-doped (436 nm) and pure (308 nm) CdO NPs. As compared to all samples, glucose-capped CdO NPs exhibited significant antibacterial activity against E. coli bacteria.
机译:通过化学沉淀法制备单相纯,Fe掺杂和葡萄糖封端的CDO纳米颗粒(NPS)。使用X射线粉末衍射(XRD),扫描电子显微镜(SEM),傅里叶变换红外(FTIR)光谱,光致发光(PL)和紫外线,研究了所有样品的结构,形态,组成,光学和发光性质,以及紫外线可见(UV-VIS)光谱。 XRD研究揭示了所有样品的单相六方晶体结构,具有P63 / MMC空间组。 SEM检测了所有样品的微观结构行为。还通过FTIR光谱鉴定合成样品的官能团。计算出的直接带能量值估计为纯3.65 eV的3.78eV,对于Fe掺杂,3.63eV用于葡萄糖封端的CDO NPS。根据PL研究,鉴定出葡萄糖封端的CDO NPS显示与Fe掺杂(436nm)和纯(308nm)CDO NPS比较的最强的光致发光信号(543nm)。与所有样品相比,葡萄糖封端的CDO NPS对大肠杆菌细菌表现出显着的抗菌活性。

著录项

  • 来源
    《Journal of materials science》 |2021年第3期|3920-3928|共9页
  • 作者单位

    Department of Engineering Physics AUCE (A) Andhra University Visakhapatnam India;

    Department of Engineering Physics AUCE (A) Andhra University Visakhapatnam India;

    Department of Physics Aditya College of Engineering and Technology Surampalem East Godavari District Andhra Pradesh India;

    Department of Physics Andhra University Visakhapatnam India;

    Department of Engineering Physics AUCE (A) Andhra University Visakhapatnam India;

    Vignan's Institute of Engineering for Women Visakhapatnam India;

    Department of Engineering Physics AUCE (A) Andhra University Visakhapatnam India;

    Department of Engineering Physics AUCE (A) Andhra University Visakhapatnam India;

  • 收录信息 美国《科学引文索引》(SCI);美国《工程索引》(EI);美国《生物学医学文摘》(MEDLINE);
  • 原文格式 PDF
  • 正文语种 eng
  • 中图分类
  • 关键词

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