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CuO nanoparticles: preparation, characterization, optical properties, and antibacterial activities

机译:CuO纳米粒子:制备,表征,光学性质和抗菌活性

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摘要

Firstly, new copper precursor was prepared from the mixture of Cu(CH_3COO)_2·H_2O and salicylic acid (1:1 weight ratio) ground for 5 min, and secondly, copper oxide nanoparticles were prepared by calcination of copper precursor at 500 °C and 600 °C for 1.5 h. The products were characterized by Fourier Transform infrared (FT-IR), UV-Vis and photoluminescent (PL) spectroscopy, X-ray powder diffraction (XRD), and transmission electron microscopy (TEM). The FT-IR, UV-Vis, PL, and XRD analysis confirmed the formation of CuO nanoparticles of high purity with a monoclinic structure. TEM images showed that the nanoparticles in both samples had almost similar shape with high agglomeration. The optical band gap value was estimated to be 4.5 and 4.8 eV, respectively, for the as-prepared CuO at 500 and 600 °C, using Tauc's plot. In addition, antibacterial activity against two gram-positive and two gram-negative stains were studied and the inhibition effect of the as-prepared CuO at 500 and 600 °C on gram-negative bacteria is higher than that on gram-positive bacteria.
机译:首先,通过Cu(CH_3COO)_2·H_2O和水杨酸(1:1重量比)的混合物制备新的铜前体5分钟,其次,通过在500℃下煅烧铜前体来制备氧化铜纳米粒子和600°C 1.5小时。该产品的特征在于傅里叶变换红外(FT-IR),UV-VI和光致发光(PL)光谱,X射线粉末衍射(XRD)和透射电子显微镜(TEM)。 FT-IR,UV-Vis,PL和XRD分析证实了CuO纳米颗粒的高纯度与单斜晶体结构。 TEM图像显示,两个样品中的纳米颗粒具有几乎与高聚凝聚的形状几乎相似。使用Tauc的图,分别在500和600℃下估计光带间隙值分别为4.5和4.8eV。此外,研究了针对两种革兰氏阳性和两种革兰氏阴性污渍的抗菌活性,并且在革兰氏阴性细菌上的500和600℃下的AS制备的CuO的抑制作用高于革兰氏阳性细菌。

著录项

  • 来源
    《Journal of materials science》 |2020年第14期|11949-11954|共6页
  • 作者单位

    Department of Chemistry Faculty of Science Golestan University Gorgan Iran;

    Department of Chemistry Faculty of Science Golestan University Gorgan Iran;

    Department of Chemistry Faculty of Science Golestan University Gorgan Iran;

    Institute of Physic of the Czech Academy of Sciences Na Slovance 2 Prague 182 21 Czech Republic;

    Institute of Physic of the Czech Academy of Sciences Na Slovance 2 Prague 182 21 Czech Republic;

    Department of Biology Faculty of Science Golestan University Gorgan Iran;

  • 收录信息 美国《科学引文索引》(SCI);美国《工程索引》(EI);美国《生物学医学文摘》(MEDLINE);
  • 原文格式 PDF
  • 正文语种 eng
  • 中图分类
  • 关键词

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