AbstractThe most stable and magnetic recoverable material XY2Z4(X = Zn, Y ='/> Structural, morphological and magnetic characters of PVP coated ZnFe_2O_4 nanoparticles
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Structural, morphological and magnetic characters of PVP coated ZnFe_2O_4 nanoparticles

机译:PVP包覆的ZnFe_2O_4纳米粒子的结构,形貌和磁性

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摘要

AbstractThe most stable and magnetic recoverable material XY2Z4(X = Zn, Y = Fe and Z = O) having spinel ferrite nanoparticles were synthesized by chemical co-precipitation technique using polyvinyl pyrrolidone (PVP) as the surfactant. The synthesized nanoparticles were characterized by using various characterization techniques. The X-ray diffraction (XRD) analyses revealed that, the ZnFe2O4have normal spinel structure of phase pure polycrystalline in nature. The FT-IR analysis revealed that the two prestigious vibration bands recorded near (540–550 cm−1) and (455–470 cm−1) show the presence of tetrahedral and octahedral voids in zinc ferrite. The transmission electron microscopy (TEM) photographs showed the synthesized ZnFe2O4nanoparticles are spherical in shape and has magnetic domain structure. The vibrating sample magnetometer (VSM) spectra indicated that the prepared ZnFe2O4nanoparticles exhibited super paramagnetic behavior along with high saturation magnetization at room temperature. Such synthesis ZnFe2O4nanoparticles with sympathetic size and tunable magnetic properties are used for various promising biomedical applications.
机译: 摘要 最稳定和磁性可恢复的材料XY 2 Z 4以聚乙烯吡咯烷酮(PVP)为表面活性剂,通过化学共沉淀技术合成了具有尖晶石型铁氧体纳米粒子的(X = Zn,Y = Fe和Z = O)。合成的纳米颗粒通过使用各种表征技术进行表征。 X射线衍射(XRD)分析表明,ZnFe 2 O 4 自然具有正常的尖晶石结构的相纯多晶。 FT-IR分析表明,在(540-550cm -1 )和(455-470cm -1 )附近记录的两个著名的振动带显示存在四面体铁酸锌中的八面体空隙。透射电子显微镜(TEM)照片显示,合成的ZnFe 2 O 4 纳米粒子为球形,具有磁畴结构。振动样品磁强计(VSM)光谱表明,制备的ZnFe 2 O 4 纳米粒子在室温下表现出超顺磁性能和高饱和磁化强度。具有交感尺寸和可调磁性的ZnFe 2 O 4 纳米粒子可用于各种有前途的生物医学领域。

著录项

  • 来源
    《Journal of materials science》 |2018年第3期|2151-2158|共8页
  • 作者单位

    PG & Research Department of Physics, St. Joseph’s College of Arts and Science (Autonomous);

    Department of Physics, Arignar Anna Gov. Arts College;

    PG & Research Department of Physics, St. Joseph’s College of Arts and Science (Autonomous);

    Department of Physics, Pondicherry University;

  • 收录信息 美国《科学引文索引》(SCI);美国《工程索引》(EI);美国《生物学医学文摘》(MEDLINE);
  • 原文格式 PDF
  • 正文语种 eng
  • 中图分类
  • 关键词

  • 入库时间 2022-08-17 13:43:19

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