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Isochronal annealing studies of a plastically deformed ferromagnetic metal using magnetic hysteresis measurements

机译:利用磁滞测量对塑性变形铁磁金属的等时退火研究

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摘要

An experimental study has been made of magnetic hysteresis in plastically deformed and annealed gadolinium (Gd) metal as a function of annealing temperature. Seven plastically deformed samples were annealed at temperatures ranging from 155° to 916°C; major and minor magnetic hysteresis loops of these seven samples plus one as‐deformed sample were examined. The results are discussed in terms of the recovery and recrystallization processes. The measurements of magnetic parameters clearly show three distinct regions of behavior, viz., the regions of annealing temperature Ta≪300°C, 300≪Ta≪500°C, and Ta≪500°C. These regions are identified as regions of recovery, recrystallization, and completed recrystallization plus additional grain growth, respectively. Two distinct advantages of the magnetic measurements are (i) using the magnetic measurements, it was found possible to distinguish between metallurgical processes which are not easily detectable using traditional measuring techniques, and (ii) the weak‐field magnetic parameters were found to be extremely sensitive to changes in microstructure resulting from the isochronal anneals. The weak‐field (or Rayleigh) hysteresis‐loop data are analyzed in terms of a spring model of domain‐wall pinning by defects. Good qualitative agreement is found between experimental results and predictions based upon this model.
机译:根据退火温度对塑性变形和退火的((Gd)金属的磁滞进行了实验研究。在155°至916°C的温度范围内对七个塑性变形的样品进行退火。检查了这七个样品和一个变形后样品的主磁滞和次磁滞回线。就回收和重结晶过程讨论了结果。磁参数的测量清楚地显示了三个不同的行为区域,即退火温度Ta≪300°C,300≪Ta≪500°C和Ta≪500°C的区域。这些区域分别被确定为恢复,重结晶和完全重结晶以及额外晶粒生长的区域。磁测量的两个明显优势是(i)使用磁测量,发现可以区分使用传统测量技术难以检测到的冶金过程,并且(ii)发现弱磁场磁参数非常高对等时退火引起的微观结构变化敏感。根据缺陷引起的畴壁钉扎的弹簧模型,分析了弱场(或瑞利)磁滞回线数据。在基于该模型的实验结果和预测之间找到了良好的定性一致性。

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    《Journal of Applied Physics》 |1973年第11期|共7页
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  • 收录信息 美国《科学引文索引》(SCI);美国《工程索引》(EI);美国《生物学医学文摘》(MEDLINE);
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  • 正文语种 eng
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