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Comparative study of the structural and magnetic properties of bulk and nanostructured Fe2CrAl

机译:Fe2 CrAl块状和纳米结构的结构和磁性的比较研究

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Nanostructured Fe2CrAl has been prepared by mechanical alloying using a high energy ball mill. The structural and magnetic properties of the as-milled and mechanically alloyed sample annealed in the presence of a magnetic field have been studied by means of X-ray diffractometry, 57Fe M?ssbauer spectroscopy and DC magnetization. The observed properties are compared to that of the bulk sample. The magnetic hyperfine fields are related to structural disorder. There is a very good enhancement of bulk magnetic properties in the nano-sized samples, the most notable one being a dramatic increase in the Curie temperature of these samples and are explained in terms of structural disordering and size effect.
机译:利用高能球磨机通过机械合金化制备了纳米结构的Fe2 CrAl。利用X射线衍射法,57 Fe Msssbauer光谱法和DC磁化技术研究了在磁场中退火后的经研磨和机械合金化的样品的结构和磁性。将观察到的特性与散装样品的特性进行比较。超精细磁场与结构无序有关。纳米尺寸样品中的体磁性能有非常好的增强,最显着的是这些样品的居里温度急剧升高,并根据结构无序和尺寸效应进行了解释。

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