Regioselective Synthesis of 5-(Arylsulfanyl)- and 5-(Benzylsulfanyl)-6-phenylsalicylates by One-Pot Cyclizations of 1,3-Bis(silyloxy)buta-1,3-dienes with 2-(Arylsulfanyl)- and 5-(Benzylsulfanyl)-3-ethoxy-1-phenylprop-2-en-1-ones

Olumide Fatunsin; Mohanad Shkoor; Abdolmajid Riahi; Munawar Hussain; Alexander Villinger; Christine Fischer; Peter Langer

首页> 外文期刊>Helvetica Chimica Acta >Regioselective Synthesis of 5-(Arylsulfanyl)- and 5-(Benzylsulfanyl)-6-phenylsalicylates by One-Pot Cyclizations of 1,3-Bis(silyloxy)buta-1,3-dienes with 2-(Arylsulfanyl)- and 5-(Benzylsulfanyl)-3-ethoxy-1-phenylprop-2-en-1-ones

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Regioselective Synthesis of 5-(Arylsulfanyl)- and 5-(Benzylsulfanyl)-6-phenylsalicylates by One-Pot Cyclizations of 1,3-Bis(silyloxy)buta-1,3-dienes with 2-(Arylsulfanyl)- and 5-(Benzylsulfanyl)-3-ethoxy-1-phenylprop-2-en-1-ones

机译：1，3-双（甲硅烷氧基）丁1，3-二烯与2-（芳基硫烷基）-和5-的一锅环化区域选择性合成5-（芳基硫烷基）-和5-（苄基硫烷基）-6-苯基水杨酸酯（苄基硫烷基）-3-乙氧基-1-苯基丙-2-烯-1-酮

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摘要

5-(Arylsulfanyl)-6-phenylsalicylates were prepared by one-pot cyclizations of 1,3-bis(trimethylsilyloxy)buta-1,3-dienes with 2-(arylsulfanyl)-3-ethoxy-1-phenylprop-2-en-1-ones.

机译：5-（芳基硫烷基）-6-苯基水杨酸酯是通过将1，3-双（三甲基甲硅烷氧基）丁1,3-二烯与2-（芳基硫烷基）-3-乙氧基-1-苯基丙-2-烯一锅化而制得的。 -1个

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来源
《Helvetica Chimica Acta》 |2010年第8期|p.1610-1621|共12页
作者
Olumide Fatunsin; Mohanad Shkoor; Abdolmajid Riahi; Munawar Hussain; Alexander Villinger; Christine Fischer; Peter Langer;
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作者单位

Institut für Chemie, Universitt Rostock, Albert-Einstein-Strasse 3a, DE-18059 Rostock, (fax: +49 381 4986412);

Institut für Chemie, Universitt Rostock, Albert-Einstein-Strasse 3a, DE-18059 Rostock, (fax: +49 381 4986412);

Institut für Chemie, Universitt Rostock, Albert-Einstein-Strasse 3a, DE-18059 Rostock, (fax: +49 381 4986412);

Institut für Chemie, Universitt Rostock, Albert-Einstein-Strasse 3a, DE-18059 Rostock, (fax: +49 381 4986412);

Leibniz-Institut für Katalyse e.V. an der Universitt Rostock, Albert-Einstein-Strasse 29a, DE-18059 Rostock;

Leibniz-Institut für Katalyse e.V. an der Universitt Rostock, Albert-Einstein-Strasse 29a, DE-18059 Rostock;

Institut für Chemie, Universitt Rostock, Albert-Einstein-Strasse 3a, DE-18059 Rostock, (fax: +49 381 4986412)|Leibniz-Institut für Katalyse e.V. an der Universitt Rostock, Albert-Einstein-Strasse 29a, DE-18059 Rostock;

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正文语种 eng
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关键词
Salicylates, 5-(arylsulfanyl)-6-phenyl-; Cyclization reactions; Diaryl sulfides; Silyl enol ethers; Multicomponent reactions; X-Ray crystallography;

机译：5-（芳基硫烷基）-6-苯基-水杨酸酯;环化反应;二芳基硫醚;甲硅烷基烯醇醚;多组分反应;X射线晶体学;

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1. Regioselective synthesis of 5-(arylsulfanyl)- and 5-(benzylsulfanyl)-6- phenylsalicylates by one-pot cyclizations of 1,3-bis(silyloxy)buta-1,3-dienes with 2-(arylsulfanyl)- and 5-(benzylsulfanyl)-3-ethoxy-1-phenylprop-2-en-1-ones [J] . Fatunsin O., Shkoor M., Riahi A., Helvetica chimica acta . 2010,第8期

机译：通过一锅式环合1,3-双（甲硅烷氧基）丁1,3-二烯与2-（芳基硫烷基）-和5-的5-（芳基硫烷基）-和5-（苄基硫烷基）-6-苯基水杨酸酯的区域选择性合成（苄基硫烷基）-3-乙氧基-1-苯基丙-2-烯-1-酮
2. Synthesis of 5-(Arylselanyl)-2-(arylsulfanyl)benzoates by [3+3] Cyclocondensation of 3-(Arylsulfanyl)-1-(silyloxy)buta-1,3-dienes with 2-(Arylselanyl)-3-(silyloxy)alk-2-en-1-ones [J] . Inam Iqbal, Muhammad Imran, Peter Langer Helvetica Chimica Acta . 2010,第9期

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3. Synthesis of 5-(arylselanyl)-2-(arylsulfanyl)benzoates by [3+3] cyclocondensation of 3-(arylsulfanyl)-1-(silyloxy)buta-1,3-dienes with 2-(arylselanyl)-3-(silyloxy)alk-2-en-1-ones [J] . Iqbal I., Imran M., Langer P. Helvetica chimica acta . 2010,第9期

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Regioselective Synthesis of 5-(Arylsulfanyl)- and 5-(Benzylsulfanyl)-6-phenylsalicylates by One-Pot Cyclizations of 1,3-Bis(silyloxy)buta-1,3-dienes with 2-(Arylsulfanyl)- and 5-(Benzylsulfanyl)-3-ethoxy-1-phenylprop-2-en-1-ones

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