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Influence of decreased sample size on cone calorimeter results

机译:样本量减少对锥形量热仪结果的影响

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Cone calorimeter sample size sensitivity and the influence of sample size on the results were studied in order to investigate the possibility to use smaller samples than prescribed by the standard. The influence of the position of the sample on the sample holder of the decreased samples was also studied. Samples of birch plywood, industrial two-component polyurethane adhesive and polypropylene wax were tested. The results from standard size sample experiments, 100cm~2, and decreased sample size, 50 and 25cm~2, were compared, in order to investigate the sample size influence on the results. The experiments were performed using an external heat flux of 50kW/m~2 . The results show differences between the sample types. The measured heat release rates for plywood and polyurethane adhesive indicate that the sample size is possible to down-scale, while the polypropylene wax results show the opposite. All sample types and sizes show constant results for the effective heat of combustion, indicating down-scalability. For in-house testing and screening of materials, downscaling can be used for most sample types. However, results from experiments carried out with decreased sample size should not be compared to results from experiments executed according to the standard procedure.
机译:为了研究使用比标准规定更小的样品的可能性,研究了锥形量热仪的样品敏感性和样品量对结果的影响。还研究了样品位置对减少样品的样品架的影响。测试了桦木胶合板,工业用双组分聚氨酯胶粘剂和聚丙烯蜡的样品。比较了标准大小的样本实验(100cm〜2)和减小的样本大小(50和25cm〜2)的结果,以研究样本大小对结果的影响。实验是使用50kW / m〜2的外部热通量进行的。结果显示了样本类型之间的差异。胶合板和聚氨酯粘合剂测得的放热率表明样品尺寸可能缩小,而聚丙烯蜡的结果却相反。所有样品类型和大小均显示出有效燃烧热的恒定结果,表明可缩小规模。对于内部测试和材料筛选,缩小比例可用于大多数样品类型。但是,不应将样本量减少的实验结果与根据标准程序进行的实验结果进行比较。

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