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POROSITY, CHARACTERIZATION AND STRUCTURAL PROPERTIES OF NATURAL ZEOLITE - CLINOPTILOLITE - AS A SORBENT

机译:天然沸石-斜硅沸石-吸附剂的孔隙率,表征与结构性能。

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The characterization and porous structure of raw and modified clinoptilolite as a sorbent has been investigated by nitrogen adsorption, X-ray diffraction, X-ray fluorescence, Fourier transform infrared spectroscopy, differential thermal analysis, scanning electron microscopy and atomic force microscopy methods. The nitrogen adsorption data revealed that the total pore volume and specific surface area were increased after modification. The nitrogen adsorption was used to determine percent of mesoporosity. The TG data show that 14 wt. % of clinoptilolite is lost after heating up to 1200 ℃. Two types of porosities - primary porosity (microporosity) and secondary one (meso- and macropo-rosity) have been observed.
机译:通过氮吸附,X射线衍射,X射线荧光,傅里叶变换红外光谱,差热分析,扫描电子显微镜和原子力显微镜方法研究了粗斜发沸石和改性斜发沸石作为吸附剂的表征和多孔结构。氮吸附数据表明,改性后总孔体积和比表面积增加。氮吸附用于确定介孔百分数。 TG数据显示14重量%。加热到1200℃后,损失了斜发沸石的%。已经观察到两种类型的孔隙度:主要孔隙度(微孔隙度)和次要孔隙度(中孔隙度和大孔隙度)。

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  • 来源
    《Environment protection engineering》 |2013年第1期|139-152|共14页
  • 作者单位

    Department of Environment and Energy, Science and Research Branch, Islamic Azad University,Tehran, Iran;

    Department of Environment and Energy, Science and Research Branch, Islamic Azad University,Tehran, Iran;

    Department of Chemistry, Islamic Azad University, Central Tehran Branch, Tehran, Iran;

    Department of Environment and Energy, Science and Research Branch, Islamic Azad University,Tehran, Iran;

    Iranian Mineral Processing Research Center (IMPRC), Karaj, Iran;

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