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HYDROGEN GAS SENSING OF ZnO NANOWIRES SYNTHESIS BYHYDROTHERMAL TECHNIQUE

机译:水热法合成ZnO纳米线的氢气检测

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Zinc oxide nanowires were synthesized by simple hydrothermal method at 65oC for 12hour. We have used the neutrient solution of zinc-nitrate ((Zn(NO3)2) with hexamethylenetetramine (C6H12N4) in equimolar ratio. Growth pattern of ZnO NWs were epitaxial andinvestigated by X-ray diffraction for crystal structure that shows the zinc oxide nanowiresare in hexagonal (wurtzite) structure form. UV-visible photometer spectro calculate theabsorption (amalgamation) spectrum of zinc oxide nanowires. The surface morphology ofas synthesized zinc oxide nanowires was measured by Field Emission Scanning ElectronMicroscopy (FE-SEM). The sensor manufactured by zinc oxide (ZnO) nanowires grownby hydrothermal technique was utilized for hydrogen gas sensing at 150oC for about 1000ppm concentration. The detector manufacture for hydrogen sensing shows a reversiblecycle. The affect of working temperature was also tested on hydrogen gas sensingproperties of ZnO nanowires.
机译:通过简单的水热法在65oC下合成12h合成氧化锌纳米线。我们使用了等摩尔比的硝酸锌((Zn(NO3)2)与六亚甲基四胺(C6H12N4)的中性溶液,外延生长了ZnO纳米线,并通过X射线衍射对其晶体结构进行了研究,结果表明氧化锌纳米线在六方(纤锌矿)结构形式,紫外可见光度计光谱计算氧化锌纳米线的吸收(汞齐化)光谱,用场发射扫描电子显微镜(FE-SEM)测量合成的氧化锌纳米线的表面形貌。利用水热技术制备的(ZnO)纳米线在150oC左右浓度约为1000ppm的条件下进行氢气传感,检测仪的制造显示出可逆的循环,并测试了工作温度对ZnO纳米线的氢气传感性能的影响。

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