首页> 外文期刊>Journal of biomaterials and nanobiotechnology. >Antimicrobial and Catalytic Activities of Green Synthesized Silver Nanoparticles Using Bay Laurel (&i&Laurus nobilis&/i&) Leaves Extract
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Antimicrobial and Catalytic Activities of Green Synthesized Silver Nanoparticles Using Bay Laurel (&i&Laurus nobilis&/i&) Leaves Extract

机译:使用月桂树(Laurus nobilis / i)叶提取物的绿色合成银纳米颗粒的抗菌和催化活性

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In this study, bay laurel extract (BLE) used as a reducing and capping agent for the synthesis of silver nanoparticles (AgNPs). The green-prepared AgNPs investigated using UV-visible spectroscopy, Fourier-transform infrared spectroscopy (FTIR), X-ray powder diffraction (XRD), Scanning Electron Microscopy with Energy Dispersive X-ray (SEM-EDX) and Transmission electron microscopy (TEM). Formation of AgNPs monitored at ambient temperature by a change in color from the starting solution to dark brown. Green synthesis AgNps were investigated for antimicrobial activity. The microorganisms employed were E. coli , K. pneumoniae , B. cereus , S. aureus , C. lbicans and Aspergillus. The susceptibility of microorganisms against the six AgNPs solutions was determined using the disk diffusion method. The catalytic activity of the prepared AgNPs (sample, d) for basic brown 1 dye was investigated. The results showed the characteristic surface plasmon resonance peak of the AgNPs appeared at approximately 415 - 440 nm. XRD revealed peaks at 38.2, 44.16, 64.24 and 77.22 Ɵ , and the intensity of these peaks enhanced when using microwave curing compared to ambient temperature. SEM and TEM results showed that the silver nano particles have a spherical shape and the particle size for samples is less than 34 nm. FTIR spectroscopy measurements showed the binding of organic compounds on the surface of the silver nanoparticles. Highest antibacterial activity was enhanced with increasing of AgNPs dose and with increasing of extract ration against most of microorganisms except. Removal of basic brown 1 dye by the prepared AgNPs indicated complete dye removal after 8 h.
机译:在这项研究中,月桂树提取物(BLE)用作银纳米颗粒(AgNPs)合成的还原剂和加帽剂。使用紫外可见光谱,傅立叶变换红外光谱(FTIR),X射线粉末衍射(XRD),能量色散X射线扫描电子显微镜(SEM-EDX)和透射电子显微镜(TEM)对绿色制备的AgNP进行了研究)。在室温下,通过从起始溶液到深棕色的颜色变化来监测AgNP的形成。研究了绿色合成AgNps的抗菌活性。使用的微生物是大肠杆菌,肺炎克雷伯氏菌,蜡状芽孢杆菌,金黄色葡萄球菌,白色念珠菌和曲霉。使用圆盘扩散法确定了微生物对六种AgNPs溶液的敏感性。研究了制备的AgNPs(样品d)对碱性棕1染料的催化活性。结果表明,AgNPs的特征性表面等离子体共振峰出现在大约415-440nm处。 XRD显示在38.2、44.16、64.24和77.22上的峰。 ,与环境温度相比,使用微波固化时,这些峰的强度增强。 SEM和TEM结果表明,银纳米颗粒为球形,样品的粒径小于34 nm。 FTIR光谱测量显示有机化合物在银纳米颗粒表面上的结合。随着AgNPs剂量的增加和对大多数微生物的提取率的增加,最高的抗菌活性得到增强。制备的AgNP去除碱性棕1染料表明8小时后染料完全去除。

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