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Obtaining the fine-grained silicon carbide, used in the synthesis of construction ceramics

机译:获得用于建筑陶瓷合成的细粒碳化硅

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Abstract Silicon carbide is used in the production of construction and temperature-resistant goods, capable of withstanding high mechanical and thermal loads. During recent times, silicon carbide has been frequently used in the electronics industry. Since sintered silicon carbide has increasingly been used as a replacement for metal components of various devices, the process of obtaining compact goods from silicon powder has become the defining factor in the technology used for its synthesis. The selection of conditions in which the sintering is conducted depends on granulometric structure, the form and the surface condition of the initial powder. The work consists of the synthesis of silicon carbide powder using the purified form of metallurgical silicon powder and soot. The qualities of testing samples were studied, where silicon carbide was obtained using established technology, from mechanically activated elementary, fine-grained silicon and soot, by pyrolytic synthesis. It was demonstrated that synthesis produces highly pure silicon carbide powder, (α- and β-phases) with a granulometric composition that allowed subsequent sintering to produce high quality compact goods. It was established that the content of silica in synthesized silicon carbide powder does not exceed 1–2% of the total mass.
机译:摘要碳化硅用于建筑和耐高温产品的生产,能够承受较高的机械和热负荷。近年来,碳化硅已在电子工业中频繁使用。由于烧结碳化硅已越来越多地用作各种设备的金属部件的替代品,因此从硅粉获得致密物品的过程已成为其合成技术中的决定性因素。进行烧结的条件的选择取决于粒度结构,初始粉末的形式和表面条件。该工作包括使用冶金形式的硅粉和烟灰的纯化形式合成碳化硅粉。研究了测试样品的质量,其中使用成熟技术通过热解合成从机械活化的单质硅,细粒硅和烟灰中获得碳化硅。已证明合成可以生产出具有颗粒组成的高纯度碳化硅粉末(α相和β相),从而可以进行后续烧结以生产出高质量的致密物品。已确定合成的碳化硅粉末中二氧化硅的含量不超过总质量的1-2%。

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