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Microwave pre-curing of Portland cement-steel slag powder composite for its hydration properties

机译:硅酸盐水泥-钢渣粉复合材料的微波预固化水合性能

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A comparative study was carried out between normal curing, 40 degrees C steam curing for 10 h, 80 degrees C steam curing for 4 h and microwave pre-curing for 45 min to investigate the effect of microwave pre-curing on the hydration of Portland cement-steel slag powder composite. The compressive strength of mortar prepared with composite binder was tested. The hydration and microstructure of the composite were also studied by XRD, TG-DSC, MIP, Water absorption and SEM-EDS methods. The results show that although the hydration degree of composite binder microwave treated is lower than that cured with steam, the porosity, especially the pores larger than 50 nm, is reduced significantly by microwave pre-curing. Therefore, a small amount of hydrated products can connect each phase into a whole to improve the compressive strength of mortar treated with microwave when compared with other three regimes. In addition, as for the inert RO or Fe2O3 in the steel slag, it does not have an adverse effect on the microstructure as it can be tightly connected with the hydrated gel. But microwave pre-curing cannot accelerate the hydration of C2F, which is different from 80 degrees C steam curing. (C) 2018 Elsevier Ltd. All rights reserved.
机译:在正常固化,40摄氏度蒸汽固化10小时,80摄氏度蒸汽固化4小时和微波预固化45分钟之间进行了比较研究,以研究微波预固化对硅酸盐水泥水化的影响-钢渣粉复合材料。测试了用复合粘合剂制备的砂浆的抗压强度。还通过XRD,TG-DSC,MIP,吸水率和SEM-EDS方法研究了复合材料的水合和微观结构。结果表明,虽然微波处理的复合粘合剂的水合度低于蒸汽固化的水合度,但微波预固化显着降低了孔隙率,尤其是大于50nm的孔。因此,与其他三种方式相比,少量的水合产物可以将每个相连接成一个整体,以提高用微波处理的砂浆的抗压强度。另外,对于钢渣中的惰性RO或Fe 2 O 3,由于可以与水合凝胶紧密连接,因此对显微组织没有不利影响。但是微波预固化不能促进C2F的水合,这与80摄氏度的蒸汽固化不同。 (C)2018 Elsevier Ltd.保留所有权利。

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