A rapid and efficient determination of natural estrogens in soils by pressurised liquid extraction and gas chromatography-mass spectrometry

Josefine Beck; Kai Uwe Totsche; Ingrid Koegel-Knabner

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A rapid and efficient determination of natural estrogens in soils by pressurised liquid extraction and gas chromatography-mass spectrometry

机译：加压液体萃取和气相色谱-质谱法快速有效地测定土壤中的天然雌激素

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We present a new analytical procedure for the extraction and determination of natural estrogens in soils based on pressurised liquid extraction and GC-MS determination. After testing twelve solvents, acetone proved to be the most efficient extractant. The

机译：我们提出了一种新的分析方法，用于基于加压液体萃取和GC-MS测定的土壤中天然雌激素的萃取和测定。在测试了十二种溶剂后，丙酮被证明是最有效的萃取剂。的

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来源
《Chemosphere》 |2008年第5期|p.954-960|共7页
作者
Josefine Beck; Kai Uwe Totsche; Ingrid Koegel-Knabner;
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作者单位

Lehrstuhl fuer Bodenkunde, Department fuer Oekologie, Wissenschaftszentrum Weihenstephan fur Ernaehrung, Landnutzung und Umwelt, Technische Universitaet Muenchen, D-85350 Freising- Weihenstephan, Germany;

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收录信息美国《科学引文索引》(SCI);美国《工程索引》(EI);美国《化学文摘》(CA);
原文格式 PDF
正文语种 eng
中图分类大气污染及其防治;
关键词
steroids; pressurized liquid extraction (PLE); accelerated solvent extraction (ASE); agricultural soil; soil extraction;

机译：类固醇;加压液体萃取（PLE）;加速溶剂萃取（ASE）;农业土壤;土壤萃取;

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机译：选择性加压液体萃取后填充吸附剂的微萃取用于气相色谱-质谱法测定污水污泥中的溴化二苯醚
2. Use of microextraction by packed sorbents following selective pressurised liquid extraction for the determination of brominated diphenyl ethers in sewage sludge by gas chromatography-mass spectrometry [J] . María Pilar Martínez-Moral, María Teresa Tena Journal of chromatography, A: Including electrophoresis and other separation methods . 2014,第Null期

机译：选择性加压液体萃取后填充吸附剂的微萃取用于气相色谱-质谱法测定污水污泥中的溴化二苯醚
3. Static pressurised liquid extraction of nitrated polycyclic aromatic hydrocarbons from soils with on-line filtration-preconcentration prior to gas chromatography-mass spectrometry detection [J] . J.L.Luque-Garcia, M.D.Luque de Castro The Analyst: The Analytical Journal of the Royal Society of Chemistry: A Monthly International Publication Dealing with All Branches of Analytical Chemistry . 2004,第7期

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4. Determination of estrogen-like compounds in fish liver tissue by solid-phase extraction-gas chromatography-mass spectrometry [C] . Jin Shiwei, Huang Yan, Yi Qiong 2011 International Conference on Electric Technology and Civil Engineering . 2011

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5. Determination of Polycyclic Aromatic Hydrocarbons (PAHs) in Water by Dispersive Liquid-Liquid Microextraction with Gas Chromatography-Mass Spectrometry (DLLME-GC-MS) [D] . Ogunkunle, Emmanuel O. 2018

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6. Simultaneous Determination of 13 Priority Polycyclic Aromatic Hydrocarbons in Tehran’s Tap Water and Water for Injection Samples Using Dispersive Liquid-Liquid Micro Extraction Method and Gas Chromatography-Mass Spectrometry [O] . Ramezan Sadeghi, Farzad Kobarfard, Hassan Yazdanpanah, 2016

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7. Quantitative determination of octylphenol, nonylphenol, alkylphenol ethoxylates and alcohol ethoxylates by pressurized liquid extraction and liquid chromatography-mass spectrometry in soils treated with sewage sludges [O] . Andreu Pérez, V., Ferrer, Emilia, Rubio, José Luis, 2007

机译：加压液体萃取-液相色谱-质谱法测定污水污泥处理土壤中辛基苯酚，壬基苯酚，烷基苯酚乙氧基化物和醇乙氧基化物
8. GC/MS (Gas Chromatography-Mass Spectrometry) Analysis of Organics in Drinking Water Concentrates and Advanced Waste Treatment Concentrates. Volume 3. Batch Liquid-Liquid Extraction and Analysis of 10-Liter Sample and Analysis of Concentrates from Small Volumes (10 to 50 Liters) of Drinking Water [R] . Lucas, S. V. 1984

机译：GC / ms（气相色谱 - 质谱）分析饮用水浓缩物和先进废物处理浓缩物中的有机物。第3卷。批量液 - 液萃取和分析10升样品并分析小体积（10至50升）饮用水中的浓缩物

A rapid and efficient determination of natural estrogens in soils by pressurised liquid extraction and gas chromatography-mass spectrometry

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