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Growth And Characterization Of Zno Nanostructured Thin Films By A Two Step Chemical Method

机译:两步化学法生长Zno纳米结构薄膜及其表征

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Zinc oxide (ZnO) nanostructured seed layer was grown by successive ionic layer adsorption and reaction (SILAR) method on glass substrate. The as-prepared nanostructured seed layer was characterized by X-ray diffraction (XRD) and scanning electron microscope (SEM) for its structure and surface morphology. XRD results showed (0 0 2) oriented ZnO seed layer growth. Surface morphology study revealed the cluster of ZnO nanocrystals with hexagonal shape. ZnO nanorods (NRs) have been grown over the as-prepared ZnO nanostructured seed layer using a simple chemical bath deposition (CBD) method by immersing seed layer substrate in a chemical bath. It has been found that the morphology of the nanostructured seed layer is a key influencing factor for the growth of vertical ZnO NRs. In our growth method, we were successful in growing vertical NRs with diameter of about 70-150 nm with perfect hexagonal shape. Photoluminescence (PL) and Raman studies were carried out to analyse the crystal quality of our as-grown ZnO nanorods.
机译:通过连续离子层吸附和反应(SILAR)方法在玻璃基板上生长氧化锌(ZnO)纳米结构种子层。通过X射线衍射(XRD)和扫描电子显微镜(SEM)表征所制备的纳米结构种子层的结构和表面形态。 XRD结果表明(0 0 2)取向的ZnO种子层生长。表面形态学研究揭示了具有六边形形状的ZnO纳米晶体簇。 ZnO纳米棒(NRs)已通过使用简单的化学浴沉积(CBD)方法,通过将种子层基板浸入化学浴中而在制备好的ZnO纳米结构化种子层上生长。已经发现,纳米结构种子层的形态是垂直ZnO NRs生长的关键影响因素。在我们的生长方法中,我们成功地生长了直径约为70-150 nm的完美六边形的垂直NR。进行了光致发光(PL)和拉曼研究,以分析我们所生长的ZnO纳米棒的晶体质量。

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