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Tribological characteristics of electroless Ni-P-MoS_2 composite coatings at elevated temperatures

机译:化学高温下Ni-P-MoS_2复合镀层的摩擦学特性

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摘要

Ni-P-MoS_2 composite coatings were deposited on AISI-1045 steel plate by electroless plating followed by a heat treatment at 300℃ for 2 h. The high-temperature tribological characteristics of the composite coatings were evaluated under dry sliding conditions in a tribometer with ball-on-disk configuration. The effect of the co-deposition of MoS_2 on the friction and wear behaviors of composite coatings at elevated temperature was investigated. Scanning electron microscopy was used to determine the morphology of the worn surface of composite coating. The chemical states of some typical elements on the worn surfaces were determined by X-ray photoelectron spectroscope. The results indicate that friction coefficient of the composite coatings decreases with the increase of test temperature up to 500℃, and the best tribological properties of Ni-P-MoS_2 composite coatings are achieved at 400 ℃. The worn surface of Ni-P-MoS_2 composite coatings are characterized by mild scuffing and deformation. The improvement of tribological properties of the composite coatings was attributed to the formation of the lubricious oxide film composed of oxides of Ni and Mo at high temperatures. With the test temperature increasing to 600℃, the tribological properties of the composite coating begin to deteriorate due to softening of the coating.
机译:Ni-P-MoS_2复合涂层通过化学镀在AISI-1045钢板上沉积,然后在300℃下热处理2 h。复合涂层的高温摩擦学特性是在干滑动条件下,在具有圆盘摩擦结构的摩擦计中进行评估的。研究了MoS_2共沉积对复合涂层在高温下的摩擦磨损性能的影响。使用扫描电子显微镜确定复合涂层的磨损表面的形态。用X射线光电子能谱仪测定了磨损表面上一些典型元素的化学状态。结果表明,在500℃以下,复合涂层的摩擦系数随测试温度的升高而减小,在400℃时,Ni-P-MoS_2复合涂层具有最佳的摩擦学性能。 Ni-P-MoS_2复合涂层的磨损表面具有轻度的划痕和变形。复合涂层的摩擦学性能的改善归因于在高温下形成了由Ni和Mo的氧化物组成的润滑性氧化膜。随着测试温度升高到600℃,复合涂层的摩擦学性能由于涂层的软化而开始恶化。

著录项

  • 来源
    《Applied Surface Science》 |2013年第1期|516-521|共6页
  • 作者单位

    State Key Laboratory of Solid Lubrication, Lanzhou Institute of Chemical Physics, Chinese Academy of Sciences, Lanzhou 730000, PR China;

    State Key Laboratory of Solid Lubrication, Lanzhou Institute of Chemical Physics, Chinese Academy of Sciences, Lanzhou 730000, PR China;

    State Key Laboratory of Solid Lubrication, Lanzhou Institute of Chemical Physics, Chinese Academy of Sciences, Lanzhou 730000, PR China;

    State Key Laboratory of Solid Lubrication, Lanzhou Institute of Chemical Physics, Chinese Academy of Sciences, Lanzhou 730000, PR China;

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  • 原文格式 PDF
  • 正文语种 eng
  • 中图分类
  • 关键词

    electroless; Ni-P-MoS2 composite coating; tribological characteristic; lubricious oxide film; high-temperature;

    机译:无电Ni-P-MoS2复合涂层;摩擦学特性氧化膜高温;

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