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Calcium phosphorus bio-coating on carbon/carbon composites: Preparation, shear strength and bioactivity

机译:碳/碳复合材料上的钙磷生物涂层:制备,剪切强度和生物活性

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Microwave hydrothermal (MH) combining supersonic atmospheric plasma sprayed (SAPS) calcium phosphorus (Ca-P) bio-coatings on carbon/carbon (C/C) composite has been widely used due to their osteoconductivity and osteoproductivity. However, the erratic shear strength between coatings prepared only by SAPS (outer coating) and C/C substrates has attached more attention over the implant failure. Adding a coating prepared by MH (inner coating) before SAPS can possess superior shear strength to conventional outer coating. The inner coating with fine Ca-P particles was prepared through a unique MH method under different concentrations (10, 500 and 1000 mmol/L). The influence of concentration on microstructure, phase composition, roughness and shear strength are investigated in this paper. In particularly, the roughness of inner coatings on C/C substrates was found to related to the morphologies and particle size.
机译:结合碳/碳(C / C)复合材料的超音波常压等离子体喷涂(SAPS)钙磷(Ca-P)生物涂层的微波水热(MH)由于其骨传导性和骨生产率而被广泛使用。然而,仅由SAPS(外涂层)制备的涂层与C / C基材之间不稳定的剪切强度引起了植入失败的更多关注。在SAPS之前,通过添加MH制备的涂层(内涂层)可以拥有比常规外涂层更高的剪切强度。通过独特的MH方法在不同浓度(10、500和1000 mmol / L)下制备具有细Ca-P颗粒的内涂层。研究了浓度对显微组织,相组成,粗糙度和剪切强度的影响。特别地,发现C / C基底上的内涂层的粗糙度与形态和粒度有关。

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