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ACID LEACHING STUDIES OF NEUTRON-IRRADIATED CHYRSOTILE ASBESTOS

机译:中子辐照的蛇纹石酸浸出研究

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Samples of chrysotile from Quebec (UICC B and Jeffrey 4T-30) and from the Coalinga region of California (Calidria RG-144) were irradiated with thermal neutrons in a reactor. The main activation products induced were ~46Sc, ~51Cr, ~59Fe and ~60Co. Accurately weighed samples of the irradiated materials were dispersed in N HCl by hand shaking for 10 s. After leaching for predetermined periods at 25℃, the samples were filtered and the concentrations of Mg determined in the filtrates by inductively-coupled plasma atomic emission spectrometry (IPC-AES) and the activities of the four radionuclides by high resolution γ-ray spectrometry. Similar measurements were made on solutions obtained by refluxing samples of irradiated chrysotile with 2N HCl for 2h.
机译:在反应堆中用热中子辐照魁北克(UICC B和Jeffrey 4T-30)和加利福尼亚的Coalinga地区(Calidria RG-144)的温石棉样品。诱导的主要活化产物为〜46Sc,〜51Cr,〜59Fe和〜60Co。通过手摇10秒钟,将正确称重的辐照材料样品分散在N HCl中。在25℃浸出预定时间后,将样品过滤,并通过电感耦合等离子体原子发射光谱法(IPC-AES)测定滤液中的Mg浓度,并通过高分辨率γ射线光谱法测定四种放射性核素的活性。对通过将辐照温石棉样品与2N HCl回流2小时而获得的溶液进行了类似的测量。

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