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Fabrication of Silicon Carbide Fiber-Reinforced Silicon Carbide Matrix Composites Using Binder Jetting Additive Manufacturing from Irregularly-Shaped and Spherical Powders

机译:使用不规则形状和球形粉末的粘结剂喷射添加剂制造碳化硅纤维增强的碳化硅基复合材料

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摘要

In this paper, silicon carbide fiber-reinforced silicon carbide (SiC /SiC) composites were fabricated using binder jetting additive manufacturing followed by polymer infiltration and pyrolysis. Spherical SiC powders were produced using milling, spray drying, and thermal plasma treatment, and were characterized using SEM and XRD methods. Irregularly shaped and spherical SiC powders were used to obtain SiC /SiC blends for the application in binder jetting. The effect of SiC powder shape on densification behavior, microstructure, and mechanical properties of binder jetted SiC /SiC composites was evaluated. The highest density of 2.52 g/cm was obtained after six polymer infiltration and pyrolysis cycles. The microstructure and mechanical properties of the fabricated SiC /SiC composites were characterized. Using the spherical SiC powder resulted in higher fracture toughness and hardness, but lower flexural strength compared to the irregularly shaped powder. It was shown that it is feasible to fabricate dense SiC /SiC composites using binder jetting followed by polymer infiltration and pyrolysis.
机译:在本文中,碳化硅纤维增强的碳化硅(SiC / SiC)复合材料是通过粘合剂喷射添加剂制造,随后的聚合物渗透和热解来制造的。通过研磨,喷雾干燥和热等离子处理生产球形SiC粉末,并使用SEM和XRD方法对其进行表征。使用不规则形状和球形的SiC粉末来获得SiC / SiC混合物,用于粘合剂喷射。评价了SiC粉末形状对粘合剂喷射的SiC / SiC复合材料的致密化行为,微观结构和力学性能的影响。在六个聚合物渗透和热解循环之后,获得了最高密度2.52 g / cm。表征了所制备的SiC / SiC复合材料的微观结构和力学性能。与不规则形状的粉末相比,使用球形SiC粉末可产生更高的断裂韧性和硬度,但弯曲强度更低。结果表明,通过粘合剂喷射,随后的聚合物渗透和热解来制备致密的SiC / SiC复合材料是可行的。

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