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Nondestructive determination of curcuminoids from turmeric powder using FT-NIR

机译:使用FT-NIR无损测定姜黄粉中的姜黄素

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摘要

Nondestructive method of measuring curcuminoid content of turmeric powder was developed by fourier transform near infrared (FT-NIR) spectrometer. Also, the calibration models describing the relationship between curcuminoid content and the NIR spectra of the turmeric powder were developed and evaluated. To develop the model, NIR reflectance spectra were acquired for each turmeric powder sample. Spectra were pre-processed by applying different spectra correction algorithms. The relationship between spectrometric curcuminoid content and FT-NIR spectra of turmeric powder was examined through partial least square (PLS) regression method in the wave number range of 6102 to 4246 cm−1. The root mean square error of cross-validation and test set validation were 0.104 and 0.201 whereas the determination coefficient (R2) for both the validations were 97.64 and 87.53, respectively. A low value of root mean square error and high value of R2 indicates a high correlation between the concentration and spectral data. Thus the FT-NIR offers a viable alternative to spectroscopic procedures as well as the method is time and cost effective for determination of curcuminoid content of turmeric.
机译:利用傅立叶变换近红外光谱仪(FT-NIR)开发了姜黄粉中姜黄素含量的无损检测方法。此外,开发并评估了描述姜黄素含量与姜黄粉NIR光谱之间关系的校准模型。为了建立模型,获取了每个姜黄粉样品的近红外反射光谱。通过应用不同的光谱校正算法对光谱进行了预处理。通过偏最小二乘(PLS)回归方法,在波数为6102至4246cm -1 的范围内,研究姜黄粉的光谱姜黄素含量与FT-NIR光谱之间的关系。交叉验证和测试集验证的均方根误差为0.104和0.201,而两次验证的测定系数(R 2 )分别为97.64和87.53。均方根误差的低值和R 2 的高值表示浓度与光谱数据之间的相关性高。因此,FT-NIR提供了一种可行的光谱方法替代方法,而且该方法在确定姜黄中姜黄素含量方面既省时又经济。

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