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Sagittal focusing of synchrotron radiation X-rays using a winged crystal

机译:使用翼状晶体对同步辐射X射线进行矢状聚焦

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摘要

A Si(111) winged crystal has been designed to minimize anticlastic bending and improve sagittal focusing efficiency. The crystal was thin with wide stiffening wings. The length-to-width ratio of the crystal was optimized by finite element analysis, and the optimal value was larger than the ‘golden value’. The analysis showed that the slope error owing to anticlastic bending is less than the Darwin width. The X-rays were focused two-dimensionally using the crystal and a tangentially bent mirror. The observed profiles of the focal spot agreed well with the results of a ray-tracing calculation in the energy range from 8 to 17.5 keV. X-ray diffraction measurements with a high signal-to-noise ratio using this focusing system were demonstrated for a small protein crystal.
机译:Si(111)有翼晶体已被设计为最小化抗弹性弯曲并提高弧矢聚焦效率。晶体很薄,翅膀宽而刚硬。晶体的长宽比通过有限元分析进行了优化,其最佳值大于“黄金值”。分析表明,由于反弹性弯曲而引起的倾斜误差小于达尔文宽度。使用晶体和切向弯曲的反射镜将X射线二维聚焦。在8至17.5 profileskeV的能量范围内,观察到的焦点轮廓与光线跟踪计算的结果非常吻合。使用这种聚焦系统,具有高信噪比的X射线衍射测量结果证明了对于小的蛋白质晶体。

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